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[Analysis of metribuzin and its metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry].
| Content Provider | Semantic Scholar |
|---|---|
| Author | Kai, Shigemi Akaboshi, Takeshi Waki, Masumi Fuzimaki, Teruhisa Kanazawa, Hideko |
| Copyright Year | 2011 |
| Abstract | A method for simultaneous determination of metribuzin (MET) and three metribuzin metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry (LC-MS/MS) was developed. MET and its metabolites were extracted from a sample with acetonitrile, followed by InertSepC18 and BondElut SAX cartridge cleanup. The LC separation was performed on a C18 column using 0.01 mol/L ammonium formate-acetonitrile-methanol (70 :21 : 9) as the mobile phase and MS detection with both positive and negative ion electrospray ionization. The mean recoveries from 10 livestock products and seafoods were generally >60%, and the relative standard deviations were <20% |
| Starting Page | 28 |
| Ending Page | 33 |
| Page Count | 6 |
| File Format | PDF HTM / HTML |
| Alternate Webpage(s) | https://www.jstage.jst.go.jp/article/shokueishi/52/1/52_1_28/_pdf/-char/en |
| PubMed reference number | 21383531v1 |
| Volume Number | 52 |
| Issue Number | 1 |
| Journal | Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan |
| Language | English |
| Access Restriction | Open |
| Subject Keyword | DUOXA1 gene Eluent Extraction Formates Ions Liquid Chromatography Livestock Metabolite Methanol Seafood Simple API for XML Spectrometry, Mass, Electrospray Ionization Tandem Mass Spectrometry acetonitrile formic acid, ammonium salt metribuzin sax protein, Drosophila |
| Content Type | Text |
| Resource Type | Article |
