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Magic-angle hopping as an alternative to magic-angle spinning for solid state NMR☆
| Content Provider | Semantic Scholar |
|---|---|
| Author | Szeverenyi, Nikolaus M. Bax, Adriaan Maciel, Gary E. |
| Copyright Year | 1985 |
| Abstract | Abstract A new variation is presented on the recently reported two-dimensional magic-angle hopping technique. In this new experiment, the frequency domain that provides chemical-shift anisotropy information has been “sacrificed” in favor of improved sensitivity in the isotropic chemical-shift spectrum. This is accomplished by repeatedly refocusing the initial magnetization in the t 2 (data acquisition) domain and measuring the resulting string of echoes. Although the sensitivity is still inferior to that of a standard magic-angle spinning (MAS) experiment, it far surpasses that achieved in the original 2-D approach, and may render the hopping approach an attractive alternative to MAS in some kinds of applications. |
| Starting Page | 440 |
| Ending Page | 447 |
| Page Count | 8 |
| File Format | PDF HTM / HTML |
| DOI | 10.1016/0022-2364(85)90184-2 |
| Alternate Webpage(s) | https://spin.niddk.nih.gov/bax/lit/508/49.pdf |
| Alternate Webpage(s) | https://doi.org/10.1016/0022-2364%2885%2990184-2 |
| Volume Number | 61 |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |
