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RSC Advances Vol - 2 Issue - 5

RSC Advances Vol - 2 Issue - 4

RSC Advances Vol -1

RSC Advances Vol -0

Morphology of colloidal metal pyrophosphate salts

Content Provider	Royal Society of Chemistry (RSC)
Author	Leeuwen, Y.Mikal Kegel, Willem K. Velikov, Krassimir P.
Copyright Year	2012
Abstract	We report the preparation and characterization of colloidal particles of several pyrophosphate metal salts, including, for the first time, salts containing multiple metals. These materials are compared in order to determine the influence of the composition and experimental conditions on particle morphology. From this we make two observations: first, the metal ion valence determines the degree of crystallinity of the material. While trivalent metal ions lead to amorphous precipitates, divalent ones result in crystalline nanoparticles. Furthermore, the nature of the metal ion has a significant influence on the morphology of the crystalline particles as we find clear shape preference for each metal ion. Second, methods such as autoclave treatment and surfactant addition can be used to further change particle morphology. Finally we mixed iron(III) with divalent metals during preparation and find that this only has a significant effect on the resulting particles if the FeIII : MII ratio is 1 : 5 or higher in MII content.
Starting Page	2534
Ending Page	2540
Page Count	7
File Format	HTM / HTML PDF
ISSN	20462069
Volume Number	2
Issue Number	6
Journal	RSC Advances
DOI	10.1039/c2ra00449f
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Ferric Autoclave Pyrophosphate Ion Surfactant
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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