NDLI: Alumina–titania (Al2O3–TiO2) hollow fiber sorptive microextraction coupled to inductively coupled plasma mass spectrometry for determination of trace elements in diesel and gasoline samples

Content Provider	Royal Society of Chemistry (RSC)
Author	Ngila, J. Catherine Nomngongo, Philiswa N.
Copyright Year	2015
Abstract	An alumina–titania (Al2O3–TiO2) hollow fiber membrane was synthesized using the template method coupled with a sol–gel process. The crystal forms of the mixed oxide hollow fiber was evaluated using X-ray diffraction (XRD). The morphological structure and surface characteristics of the Al2O3–TiO2 hollow fiber were characterized by scanning electron microscopy (SEM) and nitrogen adsorption/desorption BET techniques. The synthesized Al2O3–TiO2 hollow fiber membrane was combined with inductively coupled plasma mass spectrometry for on-line preconcentration and determination of trace amounts of Co, Cr, Mo, Ni, Sb and V in diesel and gasoline samples. The optimization of the experimental parameters affecting the preconcentration and determination of target analytes was performed using a full 24 factorial and central composite designs. Under optimized conditions, limits of detection (LOD) (based on the original sample) and limits of quantification (LOQ) ranged 0.1–0.9 and 0.3–3.0 ng L−1, respectively. The developed method was applied in the determination of trace elements in real diesel and gasoline samples.
Starting Page	72500
Ending Page	72507
Page Count	8
File Format	HTM / HTML PDF
ISSN	20462069
Volume Number	5
Issue Number	89
Journal	RSC Advances
DOI	10.1039/c5ra12706h
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	X-ray crystallography Factorial Hollow fiber membrane Adsorption Sol\u2013gel process Inductively coupled plasma mass spectrometry Nitrogen Scanning electron microscope Mathematical optimization
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Homogeneous liquid-liquid microextraction via flotation assistance for determination of trace amounts of manganese prior to inductively coupled plasma-mass spectrometry

Sequential cloud point extraction of trace elements from biological samples and determination by inductively coupled plasma mass spectrometry

γ-MPTMS modified nanometer-sized alumina micro-column separation and preconcentration of trace amounts of Hg, Cu, Au and Pd in biological, environmental and geological samples and their determination by inductively coupled plasma mass spectrometry

High-sensitivity microwave-induced plasma mass spectrometry for trace element analysis

Determination of arsenic in samples with high chloride content by inductively coupled plasma mass spectrometry

Inductively coupled plasma mass spectrometry of biological samples. Invited lecture

Sequential cloud point extraction of trace elements from biological samples and determination by inductively coupled plasma mass spectrometry

Evaluation of electrothermal vaporization as a sample introduction technique for the determination of trace elements in biological samples by inductively coupled plasma mass spectrometry, following dispersive liquid–liquid microextraction

Determination of Trace Elements in Ice Core Samples by Laserablation Inductively Coupled Plasma Mass Spectrometry

Alumina–titania (Al₂O₃–TiO₂) hollow fiber sorptive microextraction coupled to inductively coupled plasma mass spectrometry for determination of trace elements in diesel and gasoline samples

Similar Documents

Homogeneous liquid-liquid microextraction via flotation assistance for determination of trace amounts of manganese prior to inductively coupled plasma-mass spectrometry

Sequential cloud point extraction of trace elements from biological samples and determination by inductively coupled plasma mass spectrometry

γ-MPTMS modified nanometer-sized alumina micro-column separation and preconcentration of trace amounts of Hg, Cu, Au and Pd in biological, environmental and geological samples and their determination by inductively coupled plasma mass spectrometry

High-sensitivity microwave-induced plasma mass spectrometry for trace element analysis

Determination of arsenic in samples with high chloride content by inductively coupled plasma mass spectrometry

Inductively coupled plasma mass spectrometry of biological samples. Invited lecture

Sequential cloud point extraction of trace elements from biological samples and determination by inductively coupled plasma mass spectrometry

Evaluation of electrothermal vaporization as a sample introduction technique for the determination of trace elements in biological samples by inductively coupled plasma mass spectrometry, following dispersive liquid–liquid microextraction

Determination of Trace Elements in Ice Core Samples by Laserablation Inductively Coupled Plasma Mass Spectrometry

Alumina–titania (Al2O3–TiO2) hollow fiber sorptive microextraction coupled to inductively coupled plasma mass spectrometry for determination of trace elements in diesel and gasoline samples

Alumina–titania (Al₂O₃–TiO₂) hollow fiber sorptive microextraction coupled to inductively coupled plasma mass spectrometry for determination of trace elements in diesel and gasoline samples