NDLI: Synthesis of an electroconductive membrane using poly(hydroxymethyl-3,4-ethylenedioxythiophene-<i>co</i>-tetramethylene-<i>N</i>-hydroxyethyl adipamide)

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Back cover

Journal of Materials Chemistry C Vol - 1 Issue - 29

Journal of Materials Chemistry C Vol - 1 Issue - 19

Journal of Materials Chemistry C Vol - 1 Issue - 9

Journal of Materials Chemistry C Vol - 1 Issue - 8

Journal of Materials Chemistry C Vol - 1 Issue - 7

Journal of Materials Chemistry C Vol - 1 Issue - 6

Journal of Materials Chemistry C Vol - 1 Issue - 5

Synthesis of an electroconductive membrane using poly(hydroxymethyl-3,4-ethylenedioxythiophene-co-tetramethylene-N-hydroxyethyl adipamide)

Content Provider	Royal Society of Chemistry (RSC)
Author	Barghi, Hamidreza Taherzadeh, Mohammad J.
Copyright Year	2013
Abstract	Synthesis of a novel electroconductive membrane (ECM) was studied with the aim of producing an electroconductive membrane (ECM) with low electrical resistance and appropriate mechanical properties. The method was based on copolymerization of a highly electroconductive monomer (hydroxymethyl-3,4-ethylenedioxythiophene) with highly mechanical resistant hydrophilized polyamide 46 (polytetramethylene-N-hydroxyethyl adipamide). Due to the lack of hydroxyl groups, polyamide 46 does not have the tendency to take part in any chemical reactions, therefore prior to copolymerization, PA 46 was hydrophilized with acetaldehyde to create reactive sites, which allowed copolymerization to occur. At the final stage, a very thin layer, 566 nm conductive poly(hydroxymethyl-3,4-ethylenedioxythiophene) homopolymer was localised using in situ plasma polymerization in order to improve the electrical conductivity of the obtained copolymer. The result was an adherent, highly conductive, semi-hydrophilic and flexible ECM. The presence of hydroxyl groups in the final product led to improved hydrophilicity of the conductive membrane with a surface tension of 41 mJ m−2. The electrical resistance of PA 46 was dramatically reduced after copolymerization, to 202 in dry and 54 kΩ cm−2 in wet conditions; furthermore, after plasma treatment, this reduction continued to 105 in dry and 2 kΩ cm−2 in wet conditions. Other parameters such as flux flow, roughness, pore size, pore distribution, contact angle, surface energy and thermal stability of the ECM were also investigated.
Starting Page	6347
Ending Page	6354
Page Count	8
File Format	HTM / HTML PDF
ISSN	20507526
Volume Number	1
Issue Number	39
Journal	Journal of Materials Chemistry C
DOI	10.1039/c3tc30932k
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	PA ECM Extracellular matrix Electrical resistance and conductance Monomer Polyamide Hydroxy group Pennsylvania Route 46 Acetaldehyde Polymer Cell membrane Polymerization Electrical resistivity and conductivity Copolymer Hydrophile Surface tension Contact angle Surface energy
Content Type	Text
Resource Type	Article
Subject	Chemistry Materials Chemistry

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