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A new approach to the synthesis of molybdenum bimetallic nitrides and oxynitrides

Content Provider	Royal Society of Chemistry (RSC)
Author	Beltrán, Aurelio Beltrán, Daniel Alconchel, Silvia Sapiña, Fernando
Copyright Year	1999
Abstract	A simple processing route to molybdenum bimetallic nitrides and oxynitrides has been developed, based on the use of precursors resulting from freeze-drying of aqueous solutions of the appropriate common metal salts. Thermal decomposition of amorphous freeze-dried powders originates crystalline mixed oxides, which have been carefully characterized. Nitridation of the crystalline intermediate having Ni:Mo=2:3 metal ratio led to single-phased Ni 2 Mo 3 N. For the V-Mo-O-N system, nitridation of both amorphous and crystalline precursors results in bimetallic oxynitrides. In this way, not only the already known V 2 Mo(O x N y ) catalyst but also a new compound of different metal stoichiometry, V 3 Mo 2 (O x N y ), has been prepared. The materials have been characterized by X-ray powder diffraction, elemental analysis, scanning electron microscopy, thermogravimetry under air flow, and temperature programmed oxidation. The existence of a solid solution of stoichiometry V 1–z Mo z (O x N y ) (0≤z≤1) having rock-salt structure is discussed.
Starting Page	749
Ending Page	755
Page Count	7
File Format	PDF
ISSN	09599428
Volume Number	9
Issue Number	3
Journal	Journal of Materials Chemistry
DOI	10.1039/a808697d
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Molybdenum Freeze-drying Thermal decomposition Stoichiometry Reserve teams in Norwegian football Powder diffraction Scanning electron microscope Thermogravimetric analysis Solid solution
Content Type	Text
Resource Type	Article
Subject	Chemistry Materials Chemistry

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