NDLI: Development and preparation of lead-containing paint films and diagnostic test materials

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Journal of Environmental Monitoring Vol - 14 Issue - 4

Journal of Environmental Monitoring Vol - 14 Issue - 3

Journal of Environmental Monitoring Vol - 14 Issue - 2

Journal of Environmental Monitoring Vol -9

Journal of Environmental Monitoring Vol -8

Journal of Environmental Monitoring Vol -7

Journal of Environmental Monitoring Vol -6

Journal of Environmental Monitoring Vol -5

Journal of Environmental Monitoring Vol -4

Journal of Environmental Monitoring Vol -3

Journal of Environmental Monitoring Vol -2

Development and preparation of lead-containing paint films and diagnostic test materials

Content Provider	Royal Society of Chemistry (RSC)
Author	Salmons, Cynthia Winstead, Wayne Gutknecht, William Sorrell, Kristen Harper, Sharon L. Binstock, David Haas, Curtis McCombs, Michelle Brown, Gordon
Copyright Year	2012
Abstract	Lead in paint continues to be a threat to children's health in cities across the United States, which means there is an ongoing need for testing and analysis of paint. This ongoing analytical effort and especially development of new methods continue to drive the need for diagnostic testing materials that provide the analytical challenges of real-world paints. To this end, 31 different types of paint test materials were developed and prepared. Preparation of the materials included development of lead-containing paint films yielding an overall relative standard error for one individual test sample being less than 10%. The 31 diagnostic test materials prepared with these paint films included two lead pigments; lead concentrations from nominally 0 to 2.0 mg lead/cm2 (0 to 5% lead by weight); overlayers of both “lead-free,” oil-based and water-based paints; Al, Ba, and Mg as potential chemical interferents; red and black potential color interferents; and substrates of wood, metal, masonry, and plaster. These materials challenge each step in method development and evaluation, including paint sample collection and preparation, lead extraction, and measurement of solubilized lead. When the materials were used to test performance of a new lead-in-paint testing method based on extraction using a rotor/stator method and measurement using turbidimetry, the results agreed to within ±20% of the expected lead values for 30 out of 31 of the diagnostic test materials, thereby demonstrating their levels of quality and utility.
Starting Page	1417
Ending Page	1427
Page Count	11
File Format	HTM / HTML PDF
ISSN	14640325
Volume Number	14
Issue Number	5
Journal	Journal of Environmental Monitoring
DOI	10.1039/c2em11004k
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Ba United States Standard error Wood Stator Turbidimetry
Content Type	Text
Resource Type	Article
Subject	Public Health, Environmental and Occupational Health Management, Monitoring, Policy and Law

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