NDLI: Zeolite Socony Mobil-5 ordered mesoporous carbon as a fiber coating for solid-phase microextraction

Content Provider	Royal Society of Chemistry (RSC)
Author	Yang, Qian Wang, Zhi Gao, Wei Li, Zhi Wang, Chun Zhang, Shuaihua
Copyright Year	2015
Abstract	In this study, an ordered mesoporous carbon (OMC) with a large surface area, uniform mesoporous structure and large pore volume was synthesized by using Zeolite Socony Mobil-5 (ZSM-5) as the hard template and sucrose as the carbon precursor. The synthesized OMC-ZSM-5 was immobilized onto a stainless steel wire for the preparation of SPME fibers by a sol–gel coating method. The SPME of polycyclic aromatic hydrocarbons (PAHs) with the OMC-ZSM-5 coated fiber coupled with gas chromatography/flame ionization detection (GC/FID) provided large enhancement factors (738–2359), low limits of detection (LODs, 0.5–1.6 ng g−1) and good linearities (1.7–100.0 ng g−1) for soil samples. The relative standard deviations (RSDs) for single fiber and fiber-to-fiber reproducibilities were in the range of 4.6–7.9% and 6.1–10.2%, respectively. The developed method was successfully applied to the analysis of soil samples and the recoveries of the analytes for the method were in the range from 88.0% to 103.8%. The OMC-ZSM-5 coated fiber was stable enough for 160 extractions without a significant loss of extraction efficiency.
Starting Page	8165
Ending Page	8171
Page Count	7
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	7
Issue Number	19
Journal	Analytical Methods
DOI	10.1039/c5ay01585e
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Mesoporous material Gas chromatography OMC Sucrose Ionization Stainless steel Polycyclic aromatic hydrocarbon ZSM-5 Zeolite Carbon
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

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