NDLI: Determination of three curcuminoids in <i>Curcuma longa</i> by microemulsion electrokinetic chromatography with protective effects on the analytes

Please wait, while we are loading the content...

Spatially resolved chemical imaging of individual atmospheric particles using nanoscale imaging mass spectrometry: insight into particle origin and chemistry

Fast analysis of β-ecdysone in Brazilian ginseng (Pfaffia glomerata) extracts by high-performance liquid chromatography using a fused-core column

Quantification by SIFT-MS of volatile compounds emitted by in vitro cultures of S. aureus, S. pneumoniae and H. influenzae isolated from patients with respiratory diseases

Capillary electrophoresis of a wide range of DNA fragments in a mixed solution of hydroxyethyl cellulose

A naphthalimide-based azo colorimetric and ratiometric probe: synthesis and its application in rapid detection of cyanide anions

Determination of hepatitis B virus surface antigen in serum with a sandwich immunoassay and capillary electrophoresis–electrochemical detection

Determination of danofloxacin and its photodegradation products by HPLC-DAD. Kinetic evaluation of the degradation process and identification of photoproducts by mass spectrometry

Label-free and real-time monitoring of trypsin activity in living cells by quantum-dot-based fluorescent sensors

Hollow fiber liquid based microextraction combined with high-performance liquid-chromatography for the analysis of lidocaine in biological and pharmaceutical samples

Preparation and evaluation of vanillin molecularly imprinted polymer microspheres by reversible addition–fragmentation chain transfer precipitation polymerization

A graphene oxide-based immobilized PNGase F reagent for highly efficient N-glycan release and MALDI-TOF MS profiling

Separation and identification of curcuminoids in turmeric powder by HPLC using phenyl column

Rapid identification of black peanut seeds by confocal micro-Raman and near-infrared FT-Raman spectroscopy

In-syringe ionic liquid dispersive liquid–liquid microextraction for the determination of sulfonamides in blood using high-performance liquid chromatography

Determination of polycyclic aromatic hydrocarbons in water samples by temperature-controlled ionic liquid dispersive liquid–liquid microextraction combined with high performance liquid chromatography

Detection of immunoglobulin G based on nanoparticle surface energy transfers from fluorescein isothiocyanate to gold nanoparticles

Determination of three curcuminoids in Curcuma longa by microemulsion electrokinetic chromatography with protective effects on the analytes

Chemical composition of the essential oils from the hulls of Pistacia vera L. by using magnetic nanoparticle-assisted microwave (MW) distillation: comparison with routine MW and conventional hydrodistillation

Colorimetric copper(ii) ion sensor based on the conformational change of peptide immobilized onto the surface of gold nanoparticles

Determination of the contents of magnesium and potassium in rapeseeds using FTIR-PAS combined with least squares support vector machines and uninformative variable elimination

Development, evaluation and comparison of two independent sampling and analytical methods for ortho-phthalaldehyde vapors and condensation aerosols in air

A simple model for separation prediction of comprehensive two-dimensional gas chromatography and its applications in petroleum analysis

Highly sensitive spectrofluorimetric method for the determination of two antimigraine drugs in their tablets and in biological fluids. Application to content uniformity testing

Rapid identification of H5 avian influenza virus in chicken throat swab specimens using microfluidic real-time RT-PCR

A single cataluminescence sensor for wine identification by luminescent response profiles

Rapid biosensing of Staphylococcus aureus bacteria in milk

Rhodamine-labelled simple architectures for fluorometric and colorimetric sensing of Hg²⁺ and Pb²⁺ ions in semi-aqueous and aqueous environments

Fast preparation of a hydrophobic monolith by redox initiation and its application in the separation of small molecules

A XANES study of chromophores: the case of black glass

Pharmacokinetics and tissue distribution of a M1 muscarinic acetylcholine receptor positive allosteric potentiator, benzyl quinolone carboxylic acid

A parallel model of independent component analysis constrained by a 5-parameter reference curve and its solution by multi-target particle swarm optimization

A nitrogen-doped carbon dot/ferrocene@β-cyclodextrin composite as an enhanced material for sensitive and selective determination of uric acid

Predicting putative adverse drug reaction related proteins based on network topological properties

Purity determination and uncertainty evaluation of a new certified reference material of Pinocembrin

Simultaneous determination of antihistamine anti-allergic drugs, cetirizine, domperidone, chlorphenamine maleate, loratadine, meclizine and buclizine in pharmaceutical formulations, human serum and pharmacokinetics application

Application of l-cysteine capped core–shell CdTe/ZnS nanoparticles as a fluorescence probe for cephalexin

Viagra® and Cialis® blister packaging fingerprinting using Fourier transform infrared spectroscopy (FTIR) allied with chemometric methods

Electrochemical detection of guaiacol in bamboo juice based on the enhancement effect of RGO nanosheets

¹H NMR based metabolic profiling of the processing effect on Rehmanniae Radix

A sequential injection lab-at-valve (SI-LAV) platform for hydride generation atomic absorption spectrometry (HG-AAS): on-line determination of inorganic arsenic

Determination of trace rutin based on the surface plasmon resonance absorption of silver nanoparticles

Solid phase microextraction using a graphene composite-coated fiber coupled with gas chromatography for the determination of acetanilide herbicides in water samples

A simple and effective method for picking training samples in neural networks

Determination of pretilachlor in soil and rice using matrix solid-phase dispersion extraction by capillary electrophoresis with field amplified sample injection and electrochemiluminescence detection

Fast screening of the main phenolic acids with antioxidant properties in common spices using on-line HPLC/UV/DPPH radical scavenging assay

Quantitative analysis and stability of the rodenticide TETS (tetramine) in finished tap water

Certification of water content in NMIJ CRM 4222-a, water standard solution 0.1 mg g⁻¹, by coulometric and volumetric Karl Fischer titration

Back cover

Analytical Methods Vol - 6 Issue - 7

Analytical Methods Vol - 6 Issue - 6

Analytical Methods Vol - 6 Issue - 5

Analytical Methods Vol - 6 Issue - 4

Analytical Methods Vol - 6 Issue - 3

Analytical Methods Vol -5

Analytical Methods Vol -4

Analytical Methods Vol -3

Analytical Methods Vol -2

Analytical Methods Vol -1

Determination of three curcuminoids in Curcuma longa by microemulsion electrokinetic chromatography with protective effects on the analytes

Content Provider	Royal Society of Chemistry (RSC)
Author	Liu, Rui Xia, Zhining Chen, Cheng Li, Feng Yang, Fengqing Xiao, Wen
Copyright Year	2014
Abstract	Alkaline degradation of curcuminoids was observed when they were exposed to alkaline solution, which usually occurs during capillary electrophoresis (CE) analysis with alkaline buffers. In the present study, the stability of curcuminoids (curcumin, demethoxycurcumin, bis-demethoxycurcumin) in different solutions (a boric acid buffer, a microemulsion with n-octane as the oil phase and a boric acid buffer, and a microemulsion with an ionic liquid [BMIM]PF6 as the oil phase and a boric acid buffer) was investigated. The results indicated that the microemulsion systems have a significant protective effect on the analytes, even under alkaline conditions. Compared to the boric acid buffer only, the microemulsion with an ionic liquid showed the best protective effect. Therefore, a stable and rapid microemulsion electrokinetic chromatography (MEEKC) method, with an ionic liquid as the oil phase, was developed for the simultaneous determination of the three curcuminoids in the rhizome (Jianghuang) and tuberous root (Yujin) of Curcuma longa. The experimental parameters, including the microemulsion compositions (surfactant, co-surfactant and oil phase), pH, concentration of borate buffer and capillary temperature, were intensively investigated. Finally, the investigated curcuminoids were well separated within 9 min, using a running buffer containing 100 mM SDS, 1.6 M n-butanol and 20 mM [BMIM]PF6 in 10 mM borate buffer at pH 10.2. The developed method was fully validated (using LOD, LOQ, intra- and inter-day precision and recovery) and successfully applied to determine the content of the investigated curcuminoids in four real samples (Yujin and Jianghuang from Chengdu and Leshan). All of the results showed that MEEKC with an ionic liquid as the oil phase should be an ideal choice for the analysis of curcuminoids by CE.
Starting Page	2566
Ending Page	2571
Page Count	6
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	6
Issue Number	8
Journal	Analytical Methods
DOI	10.1039/c3ay42106f
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Octane Acid Desmethoxycurcumin Capillary electrophoresis Surfactant Jianghuang N-Butanol Leshan Chromatography Yujin Ionic liquid Turmeric Zeta potential Chengdu Rhizome Tuber PH Curcumin Curcuma Microemulsion Borate
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Chemistry and Biological Activity of Curcuminoids from Turmeric (Curcuma longa L.) Cultivars

Turmeric (Curcuma longa L.): Chemical Components and Their Effective Clinical Applications

Determination of Curcuminoids and Their Degradation Products in Turmeric (Curcuma longa) Rhizome Herbal Products by Non-aqueous Capillary Electrophoresis with Photodiode Array Detection

Separation and identification of curcuminoids in turmeric powder by HPLC using phenyl column

Unlocking the genetic diversity of Indian turmeric (Curcuma longa L.) germplasm based on rhizome yield traits and curcuminoids

Evaluation of Curcuminoids in Turmeric Rhizome (Curcuma longa L.) Collected from Different Places in India

Biological Activity of Curcuminoids Isolated from Curcuma longa

High-speed microemulsion electrokinetic chromatography

Isolation, Purification and Identification of Curcuminoids from Turmeric (Curcuma longa L.) by Column Chromatography

Determination of three curcuminoids in Curcuma longa by microemulsion electrokinetic chromatography with protective effects on the analytes

Similar Documents

Chemistry and Biological Activity of Curcuminoids from Turmeric (Curcuma longa L.) Cultivars

Turmeric (Curcuma longa L.): Chemical Components and Their Effective Clinical Applications

Determination of Curcuminoids and Their Degradation Products in Turmeric (Curcuma longa) Rhizome Herbal Products by Non-aqueous Capillary Electrophoresis with Photodiode Array Detection

Separation and identification of curcuminoids in turmeric powder by HPLC using phenyl column

Unlocking the genetic diversity of Indian turmeric (Curcuma longa L.) germplasm based on rhizome yield traits and curcuminoids

Evaluation of Curcuminoids in Turmeric Rhizome (Curcuma longa L.) Collected from Different Places in India

Biological Activity of Curcuminoids Isolated from Curcuma longa

High-speed microemulsion electrokinetic chromatography

Isolation, Purification and Identification of Curcuminoids from Turmeric (Curcuma longa L.) by Column Chromatography

Determination of three curcuminoids in Curcuma longa by microemulsion electrokinetic chromatography with protective effects on the analytes