NDLI: Synthesis of Zeolite A Crystals in the Presence of Crystal Growth Inhibitors by Microwave-Assisted Hydrothermal Technique

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Synthesis of Zeolite A Crystals in the Presence of Crystal Growth Inhibitors by Microwave-Assisted Hydrothermal Technique

Content Provider	The American Society of Mechanical Engineers (ASME) Digital Collection
Author	Baig, Mirza Aqeel Laoui, Tahar Fadhillah, Farid Muraza, Oki Khan, Zafarullah
Copyright Year	2011
Abstract	Zeolite A crystals were synthesized at 100°C from sodium metasilicate and aluminium foil by microwave assisted hydrothermal technique. It was confirmed by using X-ray diffraction technique that zeolite A was produced. The influence of heating rate on the zeolite crystal size was investigated using 2.5°C/min, 7.5°C/min, and 50°C/min. It was shown that the low heating rate resulted in larger crystal size with high crystallinity. To evaluate the effect of crystal growth inhibitors (GCIs) on the zeolite synthesis and crystal size, three types of CGIs, namely Poly Ethylene Glycol (PEG); Poly Ethylene Glycol-Methyl Ether (PEG-ME); and Brij-96, were utilized. It was found that PEG gave the best result in terms of zeolite size compared to the other two CGIs by resulting in reduction of the size of zeolite A crystals into about half compared to that without CGI.
Starting Page	775
Ending Page	779
Page Count	5
File Format	PDF
ISBN	9780791854877
DOI	10.1115/IMECE2011-63655
Volume Number	Volume 1: Advances in Aerospace Technology; Energy Water Nexus; Globalization of Engineering; Posters
Conference Proceedings	ASME 2011 International Mechanical Engineering Congress and Exposition
Language	English
Publisher Date	2011-11-11
Publisher Place	Denver, Colorado, USA
Access Restriction	Subscribed
Subject Keyword	Crystal growth Sodium Heating Aluminum Crystals X-ray diffraction Ethers (class of compounds) Microwaves
Content Type	Text
Resource Type	Article

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