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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Cielecka-Piontek, J. Jelinska, A. |
| Description | Country affiliation: Poland Author Affiliation: Cielecka-Piontek J ( Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Poznan University of Medical Sciences, Grunwaldzka 6, 60-780 Poznan, Poland. jpiontek@ump.edu.pl) |
| Abstract | A spectrophotometric method was developed for the quantitative determination of doripenem in pharmaceutical dosage form (DORIBAX) in the presence of its degradation products. The first-derivative with or without the substration technique, depending on formed products degradation was applied (lambda=324 nm). The method was linear in the range concentration (0.42-11.30)x10(-2)mg L(-1) (r=0.9981), the limits of detection and quantification were 7.60 and 45.0 microg L(-1), respectively. Recovery of doripenem ranged from 99.85 to 102.97% in pharmaceutical dosage form. This method had a good precision (RDS from 0.35 to 2.93%). The observed rate constants for doripenem degradation were comparable to those obtained in recommended HPLC method. |
| ISSN | 13861425 |
| Issue Number | 2 |
| Volume Number | 77 |
| e-ISSN | 18733557 |
| Journal | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2010-10-01 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Carbapenems Chemistry Metabolism Spectrophotometry, Ultraviolet Methods Calibration Limit Of Detection Molecular Structure Pharmaceutical Preparations Solutions Standards Water Journal Article Discipline Spectroscopy |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation |
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