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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Ajibade, Peter A. Ejelonu, Benjamin C. |
| Description | Country affiliation: South Africa Author Affiliation: Ajibade PA ( Department of Chemistry, University of Fort Hare, Private Bag X1314, Alice 5700, South Africa. pajibade@ufh.ac.za) |
| Abstract | Zn(II), Cd(II) and Hg(II) dithiocarbamate complexes have been synthesized and characterized by elemental analysis, thermogravimetric analysis, UV-Vis, FTIR, (1)H- and (13)C NMR spectroscopy. The complexes were thermolysed at 180 °C and used as single molecule precursors for the synthesis of HDA capped ZnS, CdS and HgS nanoparticles and polymethylmethacrylate (PMMA) nanocomposites. The optical and structural properties of the nanoparticles and nanocomposites were studied by UV-Vis, PL, XRD and SEM. The crystallites sizes of the nanoparticles varied between 3.03 and 23.45 nm. SEM and EDX analyses of the nanocomposites confirmed the presence of the nanoparticles in the polymer matrix. |
| ISSN | 13861425 |
| Volume Number | 113 |
| e-ISSN | 18733557 |
| Journal | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2013-09-01 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Ditiocarb Chemistry Chemical Synthesis Metal Nanoparticles Metals Nanocomposites Sulfides Coordination Complexes Crystallization Electrons Magnetic Resonance Spectroscopy Ultrastructure Optical Phenomena Particle Size Polymethyl Methacrylate Spectrometry, Fluorescence Spectroscopy, Fourier Transform Infrared Thermogravimetry X-ray Diffraction Journal Article Research Support, Non-u.s. Gov't Discipline Spectroscopy |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation |
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