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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Issa, Y. M. Shehab, Ola R. Ibrahim, H. |
| Description | Country affiliation: Egypt Author Affiliation: Ibrahim H ( Chemistry Department, Faculty of Science, Cairo University, Cairo, Egypt.) |
| Abstract | New polymeric membrane (PME), modified carbon paste (MCPE), and coated wire (CWE) selenite ion-selective electrodes based on 5,10,15,20-tetrakis-(4-methoxyphenyl)-21H,23H-porphyrin-Co(II) (CoTMeOPP) are reported. The best composition was the electrode containing 2% CoTMeOPP as the active material and 49% TCP as plasticizer. The electrodes reveal a Nernstian behavior over a concentration range of 5.5x10(-5) to 1.1x10(-2) M for PME, 5.2x10(-5) to 1.2x10(-2) M for MCPE and 1.2x10(-4) to 4.4x10(-3) M for CWE. The potentiometric response is pH dependent, since selenous acid is a diprotic acid. The slope of the selenite PVC electrode was -57.0 mV for the monovalent anion at pH 6.47, and -26.0 mV for the divalent anion at pH 11.00. The detection limits were 3.4x10(-5) and 4.7x10(-5) M at pH values 6.47 and 11.00, respectively. The electrodes manifest advantages of low resistance, very short response time (15 s), and most importantly good selectivities relative to a wide variety of other anions. In fact, the proposed selenite ion-selective electrodes show a great improvement compared to previously reported electrodes for selenite ion. The electrode was used for the determination of selenite in selenite/selenate mixture, in sodium selenite raw material powder, and in VitaFit Selenium ACE antioxidant tablets with recovery ranges of 90.0-103.3%. |
| ISSN | 03043894 |
| Issue Number | 1-3 |
| Journal | Journal of Hazardous Materials |
| Volume Number | 181 |
| e-ISSN | 18733336 |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2010-09-15 |
| Publisher Place | Netherlands |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Cobalt Ion-selective Electrodes Standards Porphyrins Sodium Selenite Analysis Hydrogen-ion Concentration Journal Article Discipline Environmental Science Discipline Environmental Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Environmental Chemistry Pollution Waste Management and Disposal Health, Toxicology and Mutagenesis Environmental Engineering |
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