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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Sladkov, Vladimir |
| Description | Country affiliation: France Author Affiliation: Sladkov V ( CNRS, Institut de Physique Nucléaire (IPN), UMR 8608, Orsay F-91406, France. sladkov@ipno.in2p3.fr) |
| Abstract | The influence of non-thermostated capillary inlet on accuracy of data obtained by affinity capillary electrophoresis is examined in the case of kinetically labile systems (with fast kinetics of equilibrium) at different temperatures. The system uranyl-selenate is studied in aqueous perchloric acid solutions (pH 2.5, ionic strength 0.05 mol l(-1)) in the temperature range from 15 °C to 55 °C. Moving of the sample through the non-thermostated inlet into the thermostated region of the capillary is used in order to avoid the influence of non efficiently thermostated short capillary inlet. The data on mobility values of uranyl and the values of stability constants obtained by this mode are compared with the data obtained in a traditionally used mode (injection in non-thermostated inlet region). The uranyl mobility values obtained by the two methods are different at temperature higher than 35 °C. However, the difference between stability constants obtained by the two methods is not significant (ambient temperature is 20 °C). |
| ISSN | 00219673 |
| Journal | Journal of Chromatography A |
| Volume Number | 1263 |
| e-ISSN | 18733778 |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2012-11-09 |
| Publisher Place | Netherlands |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Electrophoresis, Capillary Instrumentation Temperature Methods Osmolar Concentration Journal Article Discipline Analytical Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Medicine Analytical Chemistry Biochemistry |
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