NDLI: A ferrocenyl-substituted 1,2,4-triazole ligand and its $Fe^{II},$ $Ni^{II}$ and $Cu^{II}$ 1D-chain complexes

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A ferrocenyl-substituted 1,2,4-triazole ligand and its $Fe^{II},$ $Ni^{II}$ and $Cu^{II}$ 1D-chain complexes

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A ferrocenyl-substituted 1,2,4-triazole ligand and its $Fe^{II},$ $Ni^{II}$ and $Cu^{II}$ 1D-chain complexes

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Moubaraki, Boujemaa Scott, Hayley S. Bond, Alan M. Nafady, Ayman Murray, Keith S. Neville, Suzanne M. Cashion, John D.
Description	Author Affiliation: Scott HS ( School of Chemistry, Monash University, Building 23, Clayton, Victoria 3800, Australia.)
Abstract	As part of a program aimed at making bifunctional iron(II) spin-crossover (SCO) materials, particularly those having redox/ electron transfer as the second function, we have made the new ferrocene - triazole ligand ATF ([(4H-1,2,4-triazol-4-yl)amino]methylferrocene), (1), and a series of M(II) complexes of this ligand with emphasis on iron(II). Polynuclear 1D-chain complexes $[Fe(ATF)_{3}](Br)_{2}·0.5(H_{2}O)$ (2), $[Fe(ATF)_{3}](ClO_{4})_{2}·0.5(H_{2}O)$ (3), $[Ni(ATF)_{3}](ClO_{4})_{2}·0.5(H_{2}O)$ (4) and an analogous complex formed with a positively charged ATF ligand $[Fe(ATF^{+})_{3}](ClO_{4})_{5}$ (6) were formed as polycrystalline powders. Crystals of a mixed ATF/NCS-bridged copper(II) polymer $[Cu(ATF)_{2}(NCS)](ClO_{4})·(Et_{2}O)_{0.5}(MeCN)$ (5) were formed and structurally characterised. Magnetic and Mössbauer spectral measurements on 2, 3 and 6 indicated that SCO has not been achieved though the Mössbauer data show interesting temperature dependence for doublets of the two iron sites for complexes 2 and 3. Solid state cyclic voltammetric data on the iron(II) complexes 3 and 4 showed well defined, reversible ATF-based electrochemistry, similar to those shown by ATF in solution.
ISSN	14779226
Issue Number	28
Journal	Dalton Trans.
Volume Number	42
e-ISSN	13645447
Language	English
Publisher	Royal Society of Chemistry
Publisher Date	2013-07-28
Publisher Place	Great Britain (UK)
Access Restriction	Subscribed
Subject Keyword	Chemistry
Content Type	Text
Resource Type	Article
Subject	Inorganic Chemistry

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A ferrocenyl-substituted 1,2,4-triazole ligand and its $Fe^{II},$ $Ni^{II}$ and $Cu^{II}$ 1D-chain complexes

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