NDLI: Unique Separation Behavior of a $C_{60}$ Fullerene-Bonded Silica Monolith Prepared by an Effective Thermal Coupling Agent

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Unique Separation Behavior of a $C_{60}$ Fullerene-Bonded Silica Monolith Prepared by an Effective Thermal Coupling Agent

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Naito, Toyohiro Sano, Tomoharu Tsuzuki, Madoka Kobayashi, Hiroshi Murakami, Yoshiki Otsuka, Koji Kubo, Takuya Yan, Mingdi
Description	Author Affiliation: Kubo T ( Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510 (Japan). kubo@anchem.mc.kyoto-u.ac.jp.); Murakami Y ( Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510 (Japan).); Tsuzuki M ( Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510 (Japan).); Kobayashi H ( Shinwa Chemical Industries Ltd. 50-2 Kagekatsu-cho, Fushimi-ku, Kyoto 612-8307 (Japan).); Naito T ( Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510 (Japan).); Sano T ( Center for Environmental Measurement and Analysis, National Institute for Environmental Studies, Onogawa 16-2, Tsukuba, Ibaraki 305-8506 (Japan).); Yan M ( Department of Chemistry, University of Massachusetts Lowell, One University Ave., Lowell, MA 01854 (USA).); Otsuka K ( Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510 (Japan).)
Abstract	Herein, we report a newly developed $C_{60}$ fullerene-bonded silica monolith in a capillary with unique retention behavior due to the structure of $C_{60}$ fullerene. N-Hydroxysuccinimide (NHS)-conjugated $C_{60}$ fullerene was successfully synthesized by a thermal coupling agent, perfluorophenyl azide (PFPA), and assigned by spectroscopic analyses. Then, $NHS-PFPA-C_{60}$ fullerene was attached onto the surface of a silica monolith in a capillary. The capillary provided specific separation ability for polycyclic aromatic hydrocarbons in liquid chromatography by an effective π–π interaction. Furthermore, corannulene, which has a hemispherical structure, was selectively retained in the capillary based on the specific structural recognition due to the spherical $C_{60}$ fullerene. This is the first report revealing the spherical recognition ability by $C_{60}$ fullerene in liquid chromatographic separation.
ISSN	09476539
e-ISSN	15213765
Journal	Chemistry - A European Journal
Issue Number	50
Volume Number	21
Language	English
Publisher	Wiley-VCH;ChemPubSoc Europe
Publisher Date	2015-12-07
Publisher Place	Germany
Access Restriction	Open
Subject Keyword	Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Catalysis

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