NDLI: Study of (Cyclic Peptide)–Polymer Conjugate Assemblies by Small-Angle Neutron Scattering

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Study of (Cyclic Peptide)–Polymer Conjugate Assemblies by Small-Angle Neutron Scattering

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Koh, Ming Liang Fitzgerald, Paul A. Perrier, Sébastien Warr, Gregory G. Jolliffe, Katrina A.
Description	Author Affiliation: Koh ML ( School of Chemistry, The University of Sydney, NSW 2006, Australia.); FitzGerald PA ( Department of Chemistry, University of Warwick, Coventry, CV4 7AL, UK.); Warr GG ( School of Chemistry, The University of Sydney, NSW 2006, Australia.); Jolliffe KA ( School of Chemistry, The University of Sydney, NSW 2006, Australia.); Perrier S ( School of Chemistry, The University of Sydney, NSW 2006, Australia.)
Abstract	We present a fundamental study into the self-assembly of (cyclic peptide)–polymer conjugates as a versatile supramolecular motif to engineer nanotubes with defined structure and dimensions, as characterised in solution using small-angle neutron scattering (SANS). This work demonstrates the ability of the grafted polymer to stabilise and/or promote the formation of unaggregated nanotubes by the direct comparison to the unconjugated cyclic peptide precursor. This ideal case permitted a further study into the growth mechanism of self-assembling cyclic peptides, allowing an estimation of the cooperativity. Furthermore, we show the dependency of the nanostructure on the polymer and peptide chemical functionality in solvent mixtures that vary in the ability to compete with the intermolecular associations between cyclic peptides and ability to solvate the polymer shell.
ISSN	09476539
e-ISSN	15213765
Journal	Chemistry - A European Journal
Issue Number	51
Volume Number	22
Language	English
Publisher	Wiley-VCH;ChemPubSoc Europe
Publisher Date	2016-12-19
Publisher Place	Germany
Access Restriction	Open
Subject Keyword	Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Catalysis

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