NDLI: Westphalen’s diol diacetate: 19(10→5)-abeo-5β-cholest-9-ene-3β,6β-diyl diacetate

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Year: 2014 Volume: 70

Year: 2013 Volume: 69

Year: 2012 Volume: 68

Year: 2012 Volume: 68 Issue: Part 12

$Li_{0.17}Na_{5.83}Mo_{11}O_{36}$

$Poly[diamminedi-μ_{3}-dicyanamido-copper(II)]$

The layered polyphosphide $Ag_{3.73(4)}Zn_{2.27(4)}P_{16}$

The pyrochlore-type molybdate $Pr_{2}Mo_{1.73}Sc_{0.27}O_{7}$

$Na_{2}MoO_{2}As_{2}O_{7}$

$Poly[(μ_{3}-pyridine-4-carboxylato-κ^{3}$ O:O′:N)(pyridin-1-ium-4-carboxylato-κO)(thiocyanato-κN)cobalt(II)]

Di-μ-hydroxido-bis[dimethyl(thiocyanato-κN)tin(IV)]

catena-Poly[[[dichlorido(pyridin-1-ium-3-yl)arsenic(III)]-μ-chlorido] monohydrate]

1-[(Z)-1-Ferrocenylethylidene]thiocarbonohydrazide

$catena-Poly[[[diaqua(1,10-phenanthroline-κ^{2}$ $N,N′)cobalt(II)]-μ-1H-benzimidazole-5,6-dicarboxylato-κ^{2}$ N $^{3}:O$ $^{6}]$ sesquihydrate}

trans-Bis(1,3-diphenylpropane-1,3-dionato)(methanol)oxidovanadium(IV) methanol disolvate

$Chlorido\{N-[(diethylamino)dimethylsilyl]anilido-κN\}(N,N,N′,N′-tetramethylethane-1,2-diamine-κ^{2}$ N,N′)iron(II)

trans-Bis[1,2-bis(diphenylphosphanyl)ethane]chlorido(ethynyl)ruthenium(II)

$(η^{6}-Benzene)dichlorido(dicyclohexylphenylphosphane)ruthenium(II)$ benzene sesquisolvate

$Trichlorido(5,5′-dimethyl-2,2′-bipyridine-κ^{2}$ N,N′)(dimethylformamide-κO)indium(III) hemihydrate

1,1′-Bis[bis(4-tert-butylphenyl)methyl]ferrocene

$(Benzoylacetonato-κ^{2}$ O,O′)dicarbonylrhodium(I)

$Poly[[μ-N,N′-bis(2-hydroxyethyl)-N,N,N′,N′-tetramethylpropane-1,3-diaminium-κ^{2}$ O:O′]tetra-μ-bromido-dibromidodimanganese(II)]

$(3-Acetyl-5-carboxylato-4-methyl-1H-pyrazol-1-ido-κ^{2}$ N $^{1},O$ $^{5})aqua[(pyridin-2-yl)methanamine-κ^{2}$ N,N′]copper(II)

Bis[O-propan-2-yl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S,S′]nickel(II)

{6,6′-Dimethoxy-2,2′-[cyclohexane-1,2-diylbis(nitrilomethanylylidene)]diphenolato}copper(II) monohydrate

$Bis\{bis[2-(diisopropylphosphanyl)phenyl]phosphanido-κ^{3}$ P,P′,P′′}chloridonickel(II)

$Dibromido(6-methyl-2,2′-bipyridine-κ^{2}$ N,N′)cobalt(II)

$Bis[2-(1H-benzimidazol-2-yl)acetato-κ^{2}$ N $^{3},O]bis(ethanol-κO)nickel(II)$

$Bis(9-allyl-6-carboxy-9H-carbazole-3-carboxylato-κ^{2}$ O $^{3},O$ $^{3′})diaquazinc$

$Bis(μ-diisopropylhydoxylaminato)-κ^{2}$ $O:N;κ^{2}$ O:O-bis[(diisopropylhydoxylaminato-κO)beryllium]

trans-Tetraaquabis[2-(4-chlorophenoxy)acetato-κO $^{1}]nickel(II)$

$Dichlorido(η^{6}-p-cymene)(ethoxydiphenylphosphane)ruthenium(II)$

$catena-Poly[[[aqua(2,2′-bipyridine-κ^{2}$ $N,N′)zinc]-μ-furan-2,5-dicarboxylato-κ^{2}$ O $^{2}:O$ $^{5}]$ dihydrate]

Bis(trimethyl-phenyl-ammonium) µ-oxalato-bis-[oxidodiperoxido-molybdate(VI)].

$catena-Poly[sodium-μ_{2}-(N,N,N′,N′-tetramethylethane-1,2-diamine)-κ^{2}$ $N:N′-sodium-bis[μ_{2}-bis(trimethylsilyl)azanido-κ^{2}$ N:N]]

1-(Ferrocen-1-ylmethyl)-3-methylimidazol-3-ium iodide

$cis-Bis\{(E)-2-[(2-fluorophenyl)iminomethyl]phenolato-κ^{2}$ $N,O\}bis(pyridine-κN)nickel(II)^{1}$

$Di-μ-bromido-bis[bromido(4,7-diphenyl-1,10-phenanthroline-κ^{2}$ N,N′)cadmium]

[Aquabis(nitrato-κO)copper(II)]-μ-{bis[5-methyl-3-(pyridin-2-yl)-1H-pyrazol-4-yl]selenide}-[diaqua(nitrato-κO)copper(II)] nitrate monohydrate

$Bis[μ-N-(tert-butyldimethylsilyl)quinolin-8-aminato-1:2κ^{2}N^{1},N^{8}:N^{8}](N,N,N′,N′-tetramethylethane-1,2-diamine-1κ^{2}N,N′)lithiumsodium$

trans-Dichloridobis[tris(4-methoxylphenyl)phosphane-κP]platinum(II) acetone disolvate

cis-Dichloridobis(2-isocyanophenyl 4-methoxybenzoate)palladium(II) chloroform monosolvate

$Poly[[hexaaquabis(μ_{3}-pyrimidine-4,6-dicarboxylato)dicalcium]$ dihydrate]

Bis{(E)-3-[2-(hydroxyimino)propanamido]-2,2-dimethylpropan-1-aminium} bis[μ-(E)-N-(3-amino-2,2-dimethylpropyl)-2-(hydroxyimino)propanamido(2−)]bis{[(E)-N-(3-amino-2,2-dimethylpropyl)-2-(hydroxyimino)propanamide]copper(II)} bis((E)-{3-[2-(hydroxyimino)propanamido]-2,2-dimethylpropyl}carbamate) acetonitrile disolvate

Bis(2-{[bis(dimethylamino)methylidene]amino-κN}benzenesulfonato-κN)copper(II)

Bis[O-methyl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S,S′]nickel(II)

Poly[[µ-aqua-diaqua-bis-(µ-furan-2,5-dicarboxyl-ato-κ(2) O (2):O (5))bis-(1,10-phenanthroline-κ(2) N,N')dicopper(II)] N,N-dimethyl-formamide monosolvate].

$[(R)-2,2-Bis(diphenylphosphanyl)-1,1′-binaphthyl-κ^{2}$ P,P′]{2-[(2R)-1,2-diamino-1-(4-methoxyphenyl)-3-methylbutyl]-5-methoxyphenyl-κC $^{1}\}hydridoruthenium(II)$ benzene monosolvate

Bis[μ-O-isopropyl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S:S′]bis{[O-isopropyl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S,S′]mercury(II)}

rac-{[2-(Diphenylthiophosphanyl)ferrocenyl]methyl}trimethylammonium iodide chloroform monosolvate

$catena-Poly[di-μ_{3}-bromido-hexa-μ_{2}-bromido-dibromidobis(O-methyl$ $pyridine-2-carboximidate-κ^{2}$ N,N′)pentamercury(II)]

$catena-Poly[[(4,4′-dimethyl-2,2′-bipyridine-κ^{2}$ N,N′)cadmium]-di-μ-bromido]

$(4,4′-Dimethyl-2,2′-bipyridine-κ^{2}$ N,N′)(dimethylformamide-κO)diiodidocadmium

$Bis[2-(\{[2-(methylsulfanyl)phenyl]imino\}methyl)phenolato-κ^{2}$ N,O]zinc chloroform disolvate

Dipyridinium $diaquabis(pyrazole-3,5-dicarboxylato-κ^{2}$ N,O)cuprate(II) dihydrate

Bis(2,4-dimethylpyridinium) tetrabromidomercurate(II)

A salen-type trinuclear $Zn_{2}Gd$ complex

Bis[O-isopropyl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S,S′]lead(II)

μ-2,5-Dihydroxyterephthalato-bis[triaqua(1,10-phenanthroline)zinc] dihydroxyterephthalate

$catena-Poly[[[diaquacopper(II)]-bis[μ-1,5-bis(1H-imidazol-1-yl)pentane-κ^{2}$ N $^{3}:N$ $^{3′}]]$ naphthalene-1,5-disulfonate]

1-Acetylthiourea-κS)bromidobis(triphenylphosphane-κP)silver(I

trans-Dichloridobis{tris[4-(trifluoromethyl)phenyl]phosphane-κP}palladium(II) dichloromethane monosolvate

$Bis(μ-4-methylbenzoato)-κ^{3}$ $O,O′:O;κ^{3}$ $O:O,O′-bis[aqua(4-methylbenzoato-κ^{2}$ O,O′)(nicotinamide-κN $^{1})cadmium]$

trans-Bis(benzyldiphenylphosphane-κP)dichloridoplatinum(II)

$cis-\{2,6-Bis[(di-tert-butylphosphanyl)methyl]cyclohexyl-κ^{3}$ P,C $^{1},P′\}chloridopalladium(II)$

catena-Poly[[aquabis[N-(pyridin-3-yl)isonicotinamide-κN $^{1}]copper(II)]-μ-fumarato-κ^{2}$ O $^{1}:O$ $^{4}]$

$(1H-Pyrazole-κN)bis(tri-tert-butoxysilanethiolato-κ^{2}$ O,S)cadmium

Bis(μ-2-carboxymethyl-2-hydroxybutanedioato)bis[diaquamanganese(II)]–1,2-bis(pyridin-4-yl)ethene–water (1/1/2)

1,5-Diphenylthiocarbazonato-κS)trimethyltin(IV

$Bis(1,10-phenanthroline-κ^{2}$ $N,N′)(sulfato-κ^{2}$ O,O′)nickel(II) butane-2,3-diol monosolvate

Bis(butane-1,4-diammonium) di-μ-oxido-bis[trifluoridooxidomolybdate(V)] monohydrate

$Pentakis(μ_{3}-N,2-dioxidobenzene-1-carboximidato)di-μ_{2}-formato-pentakis(1H-imidazole)methanolpentamanganese(III)manganese(II)–methanol–water$ (1/3.36/0.65)

Chlorido(4-methylpyridin-2-amine-κN $^{1})(2-\{[(4-methylpyridin-2-yl)imino-κN]methyl\}phenolato-κO)copper(II)$

$Tris(5,6-dimethyl-1,10-phenanthroline-κ^{2}$ N,N′)iron(II) bis(tricyanomethanide)

Di-μ-iodido-bis[(biphenyl-2-yl)(triphenylphosphane-κP)palladium(II)]

$[5-(Pyridin-2-yl)-1H-tetrazole-κ^{2}$ N $^{4},N$ $^{5}]bis(triphenylphosphane-κP)copper(I)$ tetrafluoridoborate

Bis[4-(dimethylamino)pyridinium] bis[4-(dimethylamino)pyridine-κN $^{1}]tetrakis(thiocyanato-κN)manganate(II)$

Bromidotetrakis(2-ethyl-1H-imidazole-κN $^{3})copper(II)$ bromide

Tris(thiocyanato-κN)tris(triphenylphosphine $oxide-κO)europium(III)–(nitrato-κ^{2}$ O,O′)bis(thiocyanato-κN)tris(triphenylphosphine oxide-κO)europium(III) (1/1)

Tris(thiocyanato-κN)tris(triphenylphosphine oxide-κO)terbium(III)

$[(Triethylenetetramine)copper(II)]-μ-cyanido-κ^{2}$ N:C-[bis(cyanido-κC)copper(I)]

Bis[O-propyl $(4-ethoxyphenyl)dithiophosphonato-κ^{2}$ S,S′]nickel(II)

(4-{[(Pyridin-4-yl)methylidene]amino}phenyl)ferrocene

Tetrakis(triphenylphosphane-κP)silver(I) trifluoroacetate ethanol monosolvate

Tetrakis(triphenylarsane-κAs)silver(I) trifluoroacetate hemihydrate methanol hemisolvate

$Bis\{μ-2-[(pyrimidin-2-yl)aminomethyl]phenolato\}-κ^{2}$ N $^{1}:O;κ^{2}$ O:N $^{1}-bis(\{2-[(pyrimidin-2-yl-κN)aminomethyl]phenol\}silver(I))$ dihydrate

$Poly[[[μ_{3}-(E)-N-(pyridin-4-ylmethylidene)hydroxylaminato-κ^{3}$ $O:N:N′][μ_{2}-(E)-N-(pyridin-4-ylmethylidene)hydroxylamine-κ^{2}$ N:N′][(E)-N-(pyridin-4-ylmethylidene-κN)hydroxylamine]disilver(I)] nitrate]

$(Nitrato-κ^{2}$ O,O′)bis[(E)-N-(pyridin-4-ylmethylidene-κN)hydroxyamine]silver(I)

Tris{2-[(pyrimidin-2-yl-κN)aminomethyl]phenol}silver(I) nitrate

$Dimethyl(1,10-phenanthroline-κ^{2}$ N,N′)bis(thiocyanato-κN)tin(IV)

$Di-μ_{2}-ethanolato-octamethylbis(μ-4-methyl-5-sulfanylidene-4,5-dihydro-1H-1,2,4-triazol-1-ido-κ^{2}$ N $^{1}:N$ $^{2})di-μ_{3}-oxido-tetratin(IV)$

$Di-μ_{2}-isopropanolato-octamethylbis(μ-4-methyl-5-sulfanylidene-4,5-dihydro-1H-1,2,4-triazol-1-ido-κ^{2}$ N $^{1}:N$ $^{2})di-μ_{3}-oxido-tetratin(IV)$

$Bis[μ-(E)-N-(pyridin-3-ylmethylidene)hydroxyamine]-κ^{2}$ N $^{1}:N$ $^{3};κ^{2}$ N $^{3}:N$ $^{1}-bis\{[(E)-N-(pyridin-3-ylmethylidene-κN)hydroxyamine]silver(I)\}$ dinitrate

$Di-μ_{3}-acetato-bis\{μ-6,6′-diethoxy-2,2′-[propane-1,2-diylbis(nitrilomethanylylidene)]diphenolato\}dicadmiumdisodium$ ethanol 0.67-solvate

$[μ-1,2,3,4-Tetrakis(pyridin-4-yl)butane-κ^{2}$ N $^{1}:N$ $^{4}]bis[trimethyl(thiocyanato-κN)tin(IV)]$

$Dimethylbis(2-methylquinolin-8-olato-κ^{2}$ N,O)tin(IV)

trans-Tris(4-bromophenyl)dichloridoantimony(V)

$(Nitrato-κ^{2}$ $O,O′)bis(1,10-phenanthroline-κ^{2}$ N,N′)copper(II) tricyanomethanide

$Bis(1,10-phenanthroline-κ^{2}$ N,N′)(sulfato-O)copper(II) propane-1,3-diol monosolvate

Tricarbonylbis(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)iron

Di-μ-azido-bis(μ-1,4,7,10,13,16-hexaoxacyclooctadecane)bis(5,10,15,20-tetraphenylporphyrinato)dicadmiumdisodium

$Hexacarbonyl-2κ^{3}$ $C,3κ^{3}$ $C-di-μ_{3}-sulfido-tetrakis(tetrahydrofuran-1κO)calciumdiiron(II)(Fe—Fe)$

trans-Dichloridobis{dicyclohexyl[4-(dimethylamino)phenyl]phosphane-κP}platinum(II) dichloromethane disolvate

cis-Dichloridobis(N,N,N′,N′-tetramethylethane-1,2-diamine)platinum(II)

trans-Di-μ-chlorido-bis{chlorido[tris(3,5-dimethylphenyl)phosphane-κP]palladium(II)} dichloromethane monosolvate

$Di-μ-chlorido-bis(\{8-[bis(naphthalen-1-yl)phosphanyl]naphthalen-1-yl-κ^{2}$ C $^{1},P\}palladium(II))$ dichloromethane disolvate

Bis{2-[(phenylimino)methyl]-1H-pyrrol-1-ido}palladium(II)

$Diammine\{N-[2-(hydroxyimino)propionyl]-N′-[2-(oxidoimino)propionyl]propane-1,3-diaminido-κ^{4}$ N,N′,N′′,N′′′}iron(III)

$Tris(1,10-phenanthroline-κ^{2}$ N,N′)ruthenium(II) bis(perchlorate)

$Bis(μ-4,6-dimethylpyrimidine-2-thiolato)-κ^{3}$ $N,S:S;κ^{3}$ S:N,S-bis[(triphenylphosphane-κP)silver(I)]

$μ-Carbonato-κ^{4}$ $O,O′:O′,O′′-bis\{[2′-(di-tert-butylphosphanyl)biphenyl-2-yl-κ^{2}$ P,C $^{1}]palladium(II)\}$ dichloromethane monosolvate

4-Ferrocenyl-1-methyl-3-benzoylspiro[pyrrolidine-2,11′-indeno[1,2-b]quinoxaline]

(±)-1-(1-Allyl-1H-benzimidazol-2-yl)ethanol

N′-[(E)-2-Hydroxy-5-methoxybenzylidene]-2-methoxybenzohydrazide

N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide

Tris(5-amino-1H-1,2,4-triazol-4-ium) dihydrogenphosphate hydrogenphosphate trihydrate

3-Benzoyl-1-(2-methoxyphenyl)thiourea

(25R)-16β-Acetoxy-3β-bromo-23′,26-epoxy-23′,25-dimethyl-5α-cholest-23,23′-en-6-one dichloromethane monosolvate

2-[(E)-(Pyridin-2-ylmethylidene)amino]thiophene-3-carbonitrile

(2,4,6-Trimethylphenyl){2-[N-(2,4,6-trimethylphenyl)formamido]ethyl}ammonium chloride

Ethyl 2-(3-methyl-5-sulfanylidene-4,5-dihydro-1H-1,2,4-triazol-4-yl)acetate

Bis(adeninium) bis(hydrogensulfate) sulfate

1-Methyl-4-(4-methylstyryl)pyridinium 4-methylbenzenesulfonate

Diethyl 2,6-dimethyl-4-[5-(4-methylphenyl)-1H-pyrazol-4-yl]-1,4-dihydropyridine-3,5-dicarboxylate

4-Methoxy-4-methyl-6-phenyl-1,3-diazinane-2-thione

[3-Benzoyl-2,4-bis(3-nitrophenyl)cyclobutyl](phenyl)methanone

Ethyl (Z)-2-chloro-2-[2-(4-methoxyphenyl)hydrazin-1-ylidene]acetate

Ethyl 2-cyano-5-oxo-5-(thiophen-2-yl)-3-(3,4,5-trimethoxyphenyl)pentanoate

Isopropyl 2,2-bis(4-bromophenyl)-2-hydroxyacetate

4-Methoxybenzamidinium acetate

2-(5,6-Diphenyl-1,2,4-triazin-3-yl)aniline

4-(2-Bromophenyl)-2-phenylpyrano[3,2-c]chromen-5(4H)-one

(2E)-1-Phenyl-2-[1-(2-phenylprop-2-en-1-yl)pyrrolidin-2-ylidene]ethanone

2,4-Bis(2-ethoxyphenyl)-3-azabicyclo[3.3.1]nonan-9-one

1,2-Diphenyl-1H-benzimidazole

Tetrabutylammonium 2-[2,5-dimethyl-3-(4-nitrophenyl)-2,3-dihydro-1,2,4-oxadiazolium-4-yl]nonahydro-closo-decaborate

1,3-Bis(2-anilino-2-oxoethyl)-1H-imidazol-3-ium chloride dimethylformamide monosolvate

[2,7-Dibutoxy-8-(4-fluorobenzoyl)naphthalen-1-yl](4-fluorophenyl)methanone

5-Methoxy-2-benzofuran-1(3H)-one

(2RS,5′RS)-3′,4′-Bis(4-chlorophenyl)-3,4-dihydrospiro[acridine-2,5′(4′H)-[1,2]oxazol]-1(2H)-one

$11-Hydroxy-9-[1-(4-methylphenyl)-4-oxo-3-phenylazetidin-2-yl]-18-oxo-10-oxa-2-azapentacyclo[9.7.0.0^{1,8}.0^{2,6}.0^{12,17}]octadeca-12,14,16-triene-8-carbonitrile$

5-Bromo-2-(4-methylphenyl)-3-methylsulfinyl-1-benzofuran

$17-Hydroxy-1,8-dimethyl-17-azapentacyclo[6.6.5.0^{2,7}.0^{9,14}.0^{15,19}]nonadeca-2,4,6,9(14),10,12-hexaene-16,18-dione$

N-(1,3-Thiazol-2-yl)-N′-[(thiophen-2-yl)carbonyl]thiourea hemihydrate

2-[(Adamantan-1-yl)aminomethyl]-4-chlorophenol hemihydrate

1-Benzyl-1H-benzotriazole 3-oxide monohydrate

1,2-Bis{4-[1-(anthracen-9-ylmethyl)-1H-1,2,3-triazol-4-yl]phenyl}-1,2-bis[4,5-bis(methylsulfanyl)-1,3-dithiol-2-ylidene]ethane

3-[(Furan-2-yl)carbonyl]-1-(pyrimidin-2-yl)thiourea

Dimethyl 2,6-dimethyl-4-{3-[4-(methylsulfanyl)phenyl]-1H-pyrazol-4-yl}-1,4-dihydropyridine-3,5-dicarboxylate monohydrate

Ethyl 4-oxo-8-trifluoromethyl-1,4-dihydroquinoline-3-carboxylate

2,3-Dihydro-1H-pyrrolo[1,2-a]indole-9-carbonitrile

5-[(E)-Methoxy(phenyl)methylidene]-1,3,4-triphenyl-4,5-dihydro-1H-1,2,4-triazole

N-(2-Amino-5-chlorophenyl)-2-bromobenzenesulfonamide

Piperidine-1-carboxamidinium ethyl carbonate

1-[4-(Prop-2-en-1-yloxy)benzyl]-2-[4-(prop-2-en-1-yloxy)phenyl]-1H-benzimidazole

1-Benzoyl-3-(4-chlorophenyl)thiourea dichloromethane hemisolvate

Bis{(E)-3-[(2-hydroxybenzylidene)amino]propyl}ammonium chloride

5′′-(4-Chlorobenzylidene)-1′-(4-chlorophenyl)-1′′-methyl-1′,2′,3′,5′,6′,7′,8′,8a’-octahydrodispiro[acenaphthylene-1,3′-indolizine-2′,3′′-piperidine]-2,4′′(1H)-dione

$2,8,9-Tris(2-methylpropyl)-2,5,8,9-tetraaza-1λ^{5}-phosphatricyclo[3.3.3.0^{1,5}]undecan-5-ium$ chloride dihydrate

4-Chloro-6-methoxypyrimidin-2-amine

2-Amino-5-methylpyridinium trifluoroacetate

Bis(2,6-diamino-4-chloropyrimidin-1-ium) fumarate

9,10-Diiodophenanthrene

$N-[4-(9-Chloroquino[3,2-b]benzo[1,4]thiazin-6-yl)butyl]acetamide^{1}$

2-Methyl-N-[1-(1H-pyrrol-2-yl)ethylidene]aniline

(5S,11aS)-5-Hydroperoxy-1,5,11,11a-tetrahydro[1]benzothieno[3,2-f]indolizin-3(2H)-one

Methyl $12-hydroxy-10-[1-(4-methoxyphenyl)-2-oxo-3-phenoxyazetidin-4-yl]-11-oxa-3-azahexacyclo[11.7.1.0^{2,9}.0^{2,12}.0^{3,7}.0^{17,21}]henicosa-1(20),13,15,17(21),18-pentaene-9-carboxylate$

Westphalen’s diol diacetate: 19(10→5)-abeo-5β-cholest-9-ene-3β,6β-diyl diacetate

Diethyl 3,4-dimethyl-thieno[2,3-b]thio-phene-2,5-dicarboxyl-ate.

4-Methoxybenzamidinium nitrate

(S)-(−)-1-Phenylethanaminium hexanoate

5-Cyclopentyl-2-(4-fluorophenyl)-3-isopropylsulfonyl-1-benzofuran

9-(5-Bromo-1H-indol-3-yl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione dimethyl sulfoxide monosolvate

5-Fluoro-2-(4-methylphenyl)-3-methylsulfinyl-1-benzofuran

3-Ethylsulfinyl-2-(3-fluorophenyl)-5,6-methylenedioxy-1-benzofuran

1-(1-Benzyl-1H-benzimidazol-2-yl)ethanone

$(1S,3R,8R)-2,2-Dibromo-3,7,7,10-tetramethyltricyclo[6.4.0.0^{1,3}]dodec-9-en-11-one$

4-Chloro-6-methoxypyrimidin-2-amine–succinic acid (2/1)

$4′-Methyl-1H-14′,19′-dioxa-4′-azaspiro[indole-3,5′-tetracyclo[18.4.0.0^{2,6}.0^{8,13}]tetracosane]-1′(24′),8′,10′,12′,20′,22′-hexaene-2,7′(3H)-dione$

$4′-Methyl-14′,19′-dioxa-4′-azaspiro[acenaphthylene-1,5′-tetracyclo[18.4.0.0^{2,6}.0^{8,13}]tetracosane]-1′(24′),8′,10′,12′,20′,22′-hexaene-2,7′(1H)-dione$

3-Methylbenzene-1,2-diamine

(E)-tert-Butyl 4-(N′-hydroxycarbamimidoyl)piperazine-1-carboxylate

{2,7-Dimethoxy-8-[4-(2-methylpropyl)benzoyl]naphthalen-1-yl}[4-(2-methylpropyl)phenyl]methanone

Quinolinium 8-hy-droxy-7-iodo-quinoline-5-sulfonate 0.8-hydrate.

4-Methoxybenzamidinium hydrogen oxalate monohydrate

(S,S,S,S)-Nebivolol hydrochloride hemihydrate

Pyridine-2,5-diamine.

(1R*,2S*)-N,N'-Bis[(E)-1H-pyrrol-2-yl-methyl-idene]cyclo-hexane-1,2-diamine monohydrate.

4-Phenyl-1H-1,5-benzodiazepin-2(3H)-one

5-Chloro-1-(4-methylphenylsulfonyl)-1H-indole

Morphine hydrochloride $anhydrate^{1}$

Methyl $2-(2,3,5-trimethyl-1,1-dioxo-2H-1λ^{6},2,6-thiadiazin-4-yl)benzoate$

4-Aminopyridinium 2-chloro-4-nitrobenzoate monohydrate

N-(4-Aminopyrimidin-5-yl)-4-methyl-N-(4-methylphenylsulfonyl)benzenesulfonamide

Dibenzo[b,g]indeno[1′,2′:3,4]fluoreno[1,2-d]oxonine-5,11,16,21-tetraone

3,3,6,6-Tetramethyl-9-(1-methyl-1H-indol-2-yl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione

3,5-Dibromo-2,2,6,6,7,7-hexamethyloctane-4-one

1-Allyl-6-nitro-1H-indazole

1-(10H-phenothiazin-10-yl)ethanone

6-[4-Chloro-2-(trifluoromethyl)phenyl]-3-fluoro-2-methylpyridine

1-(2-Amino-6-methylpyrimidin-4-yl)-N,N-dimethylpiperidin-4-aminium chloride

2-Amino-4,6-dimethylpyrimidin-1-ium chloride

Dicyclohexylbis(naphthalen-1-ylmethyl)phosphonium chloride chloroform disolvate

(1S*,2R*,3S*,4R*,5R*)-5-Tetradecyloxymethyl-7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylic anhydride

$2-Hydroxy-5-[(E)-2-methylbenzylidene]-8-(2-methylphenyl)-9-phenyl-3,10-diazahexacyclo[10.7.1.1^{3,7}.0^{2,11}.0^{7,11}.0^{16,20}]henicosa-1(20),12,14,16,18-pentaen-6-one$

3,3-Dinitroazetidinium chloride

6-Methyl-1,3,5-triazine-2,4-diamine butane-1,4-diol monosolvate

2-Chloro-3-(4-methylanilino)naphthalene-1,4-dione

2-(2-Hydroxypropan-2-yl)-6-(prop-2-ynyloxy)-1-benzofuran-3(2H)-one

4-{[2-(2,4-Dinitrophenyl)hydrazinylidene](phenyl)methyl}-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ethanol monosolvate

2-(3,5-Dimethyl-1H-pyrazol-1-yl)-2-hydroxyimino-N′-[1-(pyridin-2-yl)ethylidene]acetohydrazide

Methyl 4-benzyloxy-2-hydroxybenzoate

4-[(E)-2-(Pyridin-2-yl)ethenyl]pyridine–terephthalic acid (2/1)

Dabigatran etexilate tetrahydrate

(2E)-3-[4-(Benzyloxy)phenyl]-1-(2,6-dichloro-3-fluorophenyl)prop-2-en-1-one

Ethyl 4-({1-[2-(4-bromophenyl)-2-oxoethyl]-1H-1,2,3-triazol-4-yl}methoxy)-8-(trifluoromethyl)quinoline-3-carboxylate

Ethyl 3-(2-ethoxy-2-oxoethoxy)-6-(trifluoromethyl)furo[3,2-c]quinoline-2-carboxylate

(2aR*,5S*,6aS*,8aS*,E)-Ethyl 5-hydroxy-7,7,8a-trimethyl-8-oxo-2,2a,6,6a,7,8,8a,8b-octahydro-1H-pentaleno[1,6-bc]oxepine-4-carboxylate

$(1S,3R,8R)-2,2-Dibromo-10-bromomethyl-3,7,7-trimethyltricyclo[6.4.0.0^{1,3}]dodec-9-ene$

2-[5-Bromo-1-(3-chlorobenzyl)-2-methyl-1H-indol-3-yl]acetic acid

3-(4-Bromophenyl)-1-phenyl-1H-pyrazole-4-carbaldehyde

5,12-Dimethylpyrazino[1,2-a:4,5-a′]dibenzimidazole-5,12-diium dichloride dihydrate

1-[(3,5-Dimethyl-1H-pyrazol-1-yl)carbonyl]-5-methylindolizine-3-carbonitrile

Methyl 2-(3-chlorobenzamido)benzoate

(E)-3-Chloro-N′-hydroxybenzene-1-carboximidamide

(E)-3-(3,5-Dimethoxyphenyl)-1-(1-hydroxynaphthalen-2-yl)prop-2-en-1-one

Ethyl 4-(5-bromo-1H-indol-3-yl)-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

N-(4-Fluorobenzoyl)-N′,N′′-diisopropylphosphoric triamide

6-(4-Methoxyphenyl)naphtho[2,3-b][1]benzothiophene

9-(4-Methoxyphenyl)anthracene

Morpholine–4-nitrophenol (1/2)

5-[(3,5-Dichloroanilino)methyl]-N-(3,5-dichlorophenyl)-6-methyl-2-phenylpyrimidin-4-amine

(25R)-6α-Hydroxy-5α-spirostan-3β-yl tosylate

4,6-Dimethoxy-2-(methylsulfanyl)pyrimidine–4-hydroxybenzoic acid (1/1)

4-({(Z)-5-[(Z)-3-Ethoxy-4-hydroxybenzylidene]-3-methyl-4-oxo-1,3-thiazolidin-2-ylidene}amino)benzoic acid dimethylformamide monosolvate

8-Methoxy-2H-chromene-3-carbaldehyde

(Z)-Ethyl 2-chloro-2-[2-(4-methylphenyl)hydrazinylidene]acetate

(1R,3R,4R,6S)-4-(7-Methoxy-2-oxo-2H-chromen-6-yl)-1-methyl-3,6-dioxabicyclo[3.1.0]hexan-2-yl acetate

31-Benzyloxy-5,11,17,23,29-penta-tert-butylcalix[5]arene-32,33,34,35-tetraol

N-(3-Chlorophenyl)-4-nitrobenzenesulfonamide

N-(3,5-Dimethylphenyl)-4-nitrobenzenesulfonamide

N-(2,5-Dimethylphenyl)-2-nitrobenzenesulfonamide

1,3-Dibenzyl-2-(2-chlorophenyl)-4-methylimidazolidine

2,2′-[1,2-Phenylenebis(azanediyl)]diacetonitrile

4-(3-Chloro-2,2-dimethylpropanamido)benzenesulfonamide

Morpholine-4-carboxamidinium ethyl carbonate

1-Chloro-1H-1,2,3-benzotriazole

(2E)-3-(4-Bromophenyl)-1-(4,4′′-difluoro-5′-methoxy-1,1′:3′,1′′-terphenyl-4′-yl)prop-2-en-1-one

(E)-N′-(4-Methoxybenzylidene)-2-m-tolylacetohydrazide

2-(2-Nitrophenyl)acetohydrazide

2,5-Dihexylthiophene 1,1-dioxide

2-Oxo-2H-chromen-4-yl 4-methoxybenzoate

4-Methyl-2,6-bis(pyrrolidin-1-yl)pyrimidine

5-Benzoyl-2-(1H-indol-3-yl)-4-[4-(propan-2-yl)phenyl]-4,5-dihydrofuran-3-carbonitrile

2,6-Diamino-4-chloropyrimidine–benzoic acid (1/1)

2,3-Diaminopyridinium 4-methoxyquinoline-2-carboxylate

Bis(1,2,3,4-tetrahydroquinoline-1-thiocarbonyl) disulfide

N-(2-Oxo-2H-chromen-3-yl)cyclohexanecarboxamide

2,6-Dichlorophenyl 4-chlorobenzoate

4,4′-Bipyridine-1,1′-diium bis(1,3-benzothiazole-2-thiolate)

3-(4-Methoxyphenyl)-6,7-dihydro-1H-furo[3,4-c]pyran-4(3H)-one

N $^{1}-(4-Methylphenyl)piperidine-1,4-dicarboxamide$

2,5-Bis[2-({bis[3-(dimethylazaniumyl)propyl]azaniumyl}methyl)phenyl]-1,3,4-oxadiazole hexakis(perchlorate) sesquihydrate

2-Chloro-6-methylpyrimidin-4-amine

(2E)-3-(2-Bromophenyl)-1-(5-bromothiophen-2-yl)prop-2-en-1-one

Adipic acid–2,6-bis(1H-benzimidazol-2-yl)pyridine–water (1/2/4)

[2-(4-Chlorophenyl)-1,3-selenazol-4-yl]methanol

Diphenyl (isopropylamido)phosphate

1,4-Dihydrobenzo[g]quinoxaline-2,3-dione

5,10,15,20-Tetrakis(4-acetyloxyphenyl)porphyrin including an unknown solvate

5-Bromo-7-methyl-2-(4-methylphenyl)-3-methylsulfinyl-1-benzofuran

2-(4-Methylphenyl)-2-oxoethyl 3-bromobenzoate

6-Methylpyridin-2-amine

2-(4-Methylphenyl)acetohydrazide

A triclinic polymorph of methyl (3R,3′S)-1′,1′′-dimethyl-2,2′′-dioxodispiro[indoline-3,2′-pyrrolidine-3′,3′′-indoline]-4′-carboxylate

2,2′-[4-Acetyl-1,3-phenylenebis(oxy)]diacetic acid

3β-Chloro-N-methoxy-N-methylcholest-5-ene-24-carboxamide

5-(Trifluoromethoxy)isatin

3-(2-Ethyl-2-phenylhydrazin-1-ylidene)indolin-2-one

2-Amino-N,3-dimethylbenzamide

4-(5-Chloropentanamido)benzenesulfonamide

2-[(4-Bromobenzylidene)amino]ethanol

1-(4-Bromophenyl)-2-(2-chlorophenoxy)ethanone

1,5-Dibromo-2,4-dimethoxybenzene

Cyanomethanaminium perchlorate

4-[3-(4-Methylpiperidin-1-yl)propanamido]benzenesulfonamide monohydrate

N-(3,5-Dichlorophenyl)-2-nitrobenzenesulfonamide

1-(2-Chlorobenzoyl)-3-(2,3-dimethylphenyl)thiourea

Tris(naphthalen-1-yl)phosphane chloroform hemisolvate

(E)-4-(2-Chloro-1-hydroxy-2,6,6-trimethylcyclohexyl)but-3-en-2-one

1-[(1-Methyl-1H-imidazol-5-yl)methyl]-1H-indole-5-carbonitrile

3-(4-Bromophenylsulfonyl)-5-ethyl-2-methyl-1-benzofuran

rac-Ethyl(phenyl)phosphinic acid

Methyl 6-oxo-4-phenyl-2-[(Z)-2-(pyridin-2-yl)ethenyl]-1,4,5,6-tetrahydropyridine-3-carboxylate

4-Nitrophenyl 4-hydroxy-3-methylbenzoate

N,N-Bis(diphenylthiophosphinoyl)-4-ethylaniline

2,4,6-Trinitrophenyl benzoate

3-Hydroxy-2-methoxybenzamide

1,4-Dichloro-2,3-bis(chloromethyl)butane

(3aRS,7aSR)-7a-Methoxy-2-oxo-2,3,3a,4,5,6,7,7a-octahydro-1-benzofuran-4,4-dicarbonitrile

N-(2-Chlorophenyl)-4-nitrobenzenesulfonamide

N-(2-Chlorophenyl)-1-(4-chlorophenyl)formamido 3-(2-nitrophenyl)propanoate

N′-(3-Chlorobenzylidene)-4-hydroxybenzohydrazide

N,N,N′,N′-Tetramethylguanidinium tetraphenylborate

Year: 2012 Volume: 68 Issue: Part 11

Year: 2009 Volume: 66

Year: 2009 Volume: 65

Year: 2008 Volume: 65

Year: 2008 Volume: 64

Year: 2007 Volume: 64

Westphalen’s diol diacetate: 19(10→5)-abeo-5β-cholest-9-ene-3β,6β-diyl diacetate

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Meza-reyes, Socorro Bernès, Sylvain Sandoval-ramírez, Jesús Vega Báez, José Luis Ramírez Hernández, Johana
Description	Author Affiliation: Ramírez Hernández J ( Benemérita Universidad Autónoma de Puebla, Facultad de Ciencias Químicas, Ciudad Universitaria, Puebla, Pue. 72570, Mexico.)
Abstract	The structure of the title steroid [alternative name: 3β,6β-diacetoxy-5β-methyl-19-norcholest-9(10)-ene], $C_{31}H_{50}O_{4},$ confirms the generally accepted mechanism for the rearrangement of a cholestan-5α-ol derivative reported a century ago by Westphalen. The methyl group at position 10 of the starting material migrates to position 5 in the steroidal nucleus, while a $Δ^{9}$ bond is formed, as indicated by the C=C bond length of 1.347 (4) Å. The methyl transposition leaves the 5R configuration unchanged, with the methyl oriented towards the β face. During the rearrangement, the steroidal B ring experiences a conformational distortion from chair to envelope with the C atom at position 6 as the flap. In the title structure, the isopropyl group of the side chain is disordered over two positions, with occupancies of 0.733 (10) and 0.267 (10). The carbonyl O atom in the acetyl group at C3 is also disordered with an occupancy ratio of 0.62 (4):0.38 (4).
ISSN	20569890
e-ISSN	16005368
Journal	Acta Crystallographica Section E Structure Reports Online
Issue Number	Pt 12
Volume Number	68
Language	English
Publisher	IUCr/Wiley
Publisher Date	2012-12-01
Publisher Place	United States
Access Restriction	Open
Subject Keyword	Crystallography
Content Type	Text
Resource Type	Article
Subject	Chemistry Condensed Matter Physics Materials Science

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