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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Moustafa, A. M. Farag, I. S. Ahmed Tiekink, Edward R. T. Girgis, Adel S. Ramadan, A. A. |
| Description | Author Affiliation: Farag IS ( Solid State Department, Physics Division, National Research Centre, Dokki, Giza, Egypt.); Girgis AS ( Pesticide Chemistry Department, National Research Centre, Dokki, Giza 12622, Egypt.); Ramadan AA ( Physics Department, Faculty of Science, Helwan University, Helwan, Cairo, Egypt.); Moustafa AM ( Solid State Department, Physics Division, National Research Centre, Dokki, Giza, Egypt.); Tiekink ER ( Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia.) |
| Abstract | The title compound, $C_{34}H_{38}ClN_{5}O_{2},$ has spiro links connecting the pyrrolidine ring and indole residue, as well as the piperidine and pyrrolidine rings. A half-chair conformation is found for the piperidine ring with the C atom connected to the spiro-C atom lying 0.738 (4) Å out of the plane of the remaining five atoms (r.m.s. deviation = 0.0407 Å). The methylene C atom is the flap in the envelope conformation for the pyrrolidine ring. In the crystal, supramolecular chains are sustained by alternating eight-membered $\{⋯HNCO\}_{2}$ and 14-membered $\{⋯HC_{5}O\}_{2}$ synthons. Chains are connected into a three-dimensional network by (pyrrolidine-bound phenyl-methyl)C—H⋯π(pyrrolidine-bound phenyl) edge-to-face interactions. |
| ISSN | 20569890 |
| e-ISSN | 16005368 |
| Journal | Acta Crystallographica Section E Structure Reports Online |
| Issue Number | Pt 1 |
| Volume Number | 70 |
| Language | English |
| Publisher | IUCr/Wiley |
| Publisher Date | 2014-01-01 |
| Publisher Place | United States |
| Access Restriction | Open |
| Subject Keyword | Crystallography |
| Content Type | Text |
| Resource Type | Article |
| Subject | Chemistry Condensed Matter Physics Materials Science |
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