NDLI: Determination of ketotifen fumarate by capillary electrophoresis with tris(2,2'-bipyridyl) ruthenium(II) electrochemiluminescence detection.

Please wait, while we are loading the content...

Year: 2016 Volume: 31

Year: 2015 Volume: 30

Year: 2014 Volume: 29

Year: 2013 Volume: 28

Year: 2012 Volume: 27

Year: 2011 Volume: 26

Year: 2011 Volume: 26 Issue: 6

Year: 2011 Volume: 26 Issue: 5

Catalytic effect of ReAu nanoalloy on the Te particle reaction and its application to resonance scattering spectral assay of CA125

A new Pr³âº-activated molybdate-based phosphor for application to white LEDs with blue excitation.

Simple and sensitive spectrofluorimetric method for the determination of pregabalin in capsules through derivatization with fluorescamine.

Determination of ketotifen fumarate by capillary electrophoresis with tris(2,2'-bipyridyl) ruthenium(II) electrochemiluminescence detection.

Morpho-functional modifications of human neutrophils induced by aqueous cigarette smoke extract: comparison with chemiluminescence activity.

Development of chemiluminescence method for determination of 10-hydroxycamptothecin based on luminol-[Ag(HIO6)2]5â» reaction in alkaline solution.

Effect of temperature on intense green emitting Na2Ca(PO4)F:Mn²âº phosphor.

Studies on the mass and temperature dependence of lyoluminescence intensity of microcrystalline powder of KCl.

Determination of puerarin in biological samples and its application to a pharmacokinetic study by flow-injection chemiluminescence.

Capillary electrophoresis coupled with end-column electrochemiluminescence for the determination of ephedrine in human urine, and a study of its interactions with three proteins.

A flow injection chemiluminescence method for the determination of lincomycin in serum using a diperiodato-cuprate (III)-luminol system.

Fluorescence spectrometric study on the interaction of tamibarotene with bovine serum albumin.

Year: 2011 Volume: 26 Issue: 4

Year: 2011 Volume: 26 Issue: 3

Year: 2011 Volume: 26 Issue: 2

Year: 2011 Volume: 26 Issue: 1

Year: 2010 Volume: 25

Year: 2009 Volume: 24

Year: 2008 Volume: 23

Determination of ketotifen fumarate by capillary electrophoresis with tris(2,2'-bipyridyl) ruthenium(II) electrochemiluminescence detection.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Zhou, Min Li, Yu-Jie Ma, Yong-Jun Wang, Wei-Feng Mi, Juan Chen, Hui
Description	Country affiliation: China Author Affiliation: Zhou M ( College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China. mzhou8367@sina.com)
Abstract	On the basis of an europium (III)-doped Prussian blue analog film modifying platinum electrode as the working electrode, a Ru(bpy)3²âº-based electrochemiluminescence (ECL) assay coupled with capillary electrophoresis has been first established for the determination of ketotifen fumarate (KTF). Analytes were injected onto a separation capillary of 50 cm length (50 µm i.d., 360 µm o.d.) by electrokinetic injection for 10 s at 10 kV. Parameters related to the separation and detection were discussed and optimized. It was proved that 15 mM phosphate buffer at pH 8.0 could achieve the most favorable resolution, and the highest sensitivity of detection was obtained using the detection potential at 1.25 V and 5 mM Ru(bpy)3²âº in 100 mM phosphate buffer at pH 8.0 in the detection reservoir. Under the optimized conditions, the ECL intensity was in proportion to KTF concentration over the range from 3.0 × 10â»8 to 5.0 × 10â»6 g mLâ»¹ with a detection limit of 2.1 × 10â»8 g mLâ»¹ (3σ). The relative standard deviations of the ECL intensity and the migration time were 0.95 and 0.26%, respectively. The developed method was successfully applied to determine KTF contents in pharmaceuticals and human urine with recoveries between 99.5 and 107.0%.
File Format	HTM / HTML
ISSN	15227235
Issue Number	5
Volume Number	26
e-ISSN	15227243
Journal	Luminescence
Language	English
Publisher	Wiley-Blackwell
Publisher Date	2011-09-01
Publisher Place	Great Britain (UK)
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Biophysics Discipline Biochemistry 2,2'-dipyridyl Analogs & Derivatives Electrophoresis, Capillary Methods Histamine H1 Antagonists Analysis Ketotifen Luminescent Measurements Chemistry Urine Humans Sensitivity And Specificity Evaluation Studies Journal Article Research Support, Non-u.s. Gov't
Content Type	Text
Resource Type	Article
Subject	Chemistry Biophysics

Central Library (ISO-9001:2015 Certified)
Indian Institute of Technology Kharagpur
Kharagpur, West Bengal, India | PIN - 721302

See location in the Map
03222 282435
Mail: support@ndl.gov.in

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in