NDLI: $Poly[hexaaquabis(_{4}-4-carboxybenzenesulfonato)bis(_{3}-4-carboxybenzenesulfonato)calcium(II)dipotassium(I)]$

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$Poly[hexaaquabis(_{4}-4-carboxybenzenesulfonato)bis(_{3}-4-carboxybenzenesulfonato)calcium(II)dipotassium(I)]$

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Prochniak, G. Videnova-Adrabinska, V.
Description	Country affiliation: Poland Author Affiliation: Prochniak G ( Department of Chemistry, Wroclaw University of Technology, 27 Wybrzeze Wyspianskiego Street, 50-370 Wroclaw, Poland.)
Abstract	This study presents the coordination modes and crystal organization of a calcium-potassium coordination polymer, poly[hexaaquabis( $_{4}-4-carboxybenzenesulfonato-$ $^{4}$ O $^{1}:$ O $^{1`}:$ O $^{1``}:$ O $^{4})bis($ $_{3}-4-carboxybenzenesulfonato-$ $^{2}$ O $^{1}:$ O $^{1`})calcium(II)dipotassium(I)],$ [CaK $_{2}(C$ $_{7}H$ $_{5}O$ $_{5}S)$ $_{4}(H$ $_{2}O)$ $_{6}]$ $_{n},$ displaying a novel two-dimensional framework. The potassium ion is seven-coordinated by four sulfonate and one carboxyl O atom located on five different acid ligands, two of which are unique, and by two symmetry-independent water O atoms. A pair of close potassium ions share two inversion-related sulfonate O-atom sites to form a dimeric K $_{2}O$ $_{12}$ unit, which is extended into a one-dimensional array along the a-axis direction. The six-coordinate Ca $^{2+}$ ion occupies a special position ( ) at (0, , ) and is surrounded by four sulfonate O atoms from two inversion-related pairs of unique acid monoanions and by two O atoms from aqua ligands. The compound displays a layered structure, with K $_{2}O$ $_{12}$ and CaO $_{6}$ polyhedra in the layers and aromatic linkers between the layers. The three-dimensional scaffold is open, with nano-sized channels along the c axis.
File Format	HTM / HTML
e-ISSN	20532296
Journal	Acta Crystallographica Section C Crystal Structure Communications
Issue Number	Pt 8
Volume Number	65
Language	English
Publisher	IUCr/Wiley
Publisher Date	2009-08-01
Publisher Place	United States
Access Restriction	Open
Subject Keyword	Discipline Analytical Chemistry Discipline Crystallography
Content Type	Text
Resource Type	Article

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