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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Larson, Jonathan M. Bharath, Satyaveda C. Cullen, William G. Reutt-Robey, Janice E. |
| Description | Country affiliation: United States Author Affiliation: Larson JM ( Department of Physics, University of Maryland, College Park, MD, 20742-4111, USA.); Bharath SC ( Department of Chemistry & Biochemistry, University of Maryland, College Park, MD, 20742-4454, USA.); Cullen WG ( US Army Research Laboratory, Aberdeen, MD, 21005, USA.); Reutt-Robey JE ( Department of Physics, University of Maryland, College Park, MD, 20742-4111, USA.) |
| Abstract | A carbon-nanotube-enabling scanning probe technique/nanotechnology for manipulating and measuring lithium at the nano/mesoscale is introduced. Scanning Li-nanopipette and probe microscopy (SLi-NPM) is based on a conductive atomic force microscope (AFM) cantilever with an open-ended multi-walled carbon nanotube (MWCNT) affixed to its apex. SLi-NPM operation is demonstrated with a model system consisting of a Li thin film on a Si(111) substrate. By control of bias, separation distance, and contact time, attograms of Li can be controllably pipetted to or from the MWCNT tip. Patterned surface Li features are then directly probed via noncontact AFM measurements with the MWCNT tip. The subsequent decay of Li features is simulated with a mesoscale continuum model, developed here. The Li surface diffusion coefficient for a four (two) Li layer thick film is measured as D = 8 ( ± 1.2 ) × 10 − 15 $cm^{2}$ $s^{−1}$ ( D = 1.75 ( ± 0.15 ) × 10 − 15 $cm^{2}$ $s^{−1}).$ Dual-Li pipetting/measuring with SLi-NPM enables a broad range of time-dependent Li and nanoelectrode characterization studies of fundamental importance to energy-storage research. |
| File Format | HTM / HTML |
| ISSN | 16136810 |
| Issue Number | 37 |
| Journal | Small |
| Volume Number | 11 |
| e-ISSN | 16136829 |
| Language | English |
| Publisher | Wiley-VCH |
| Publisher Date | 2015-10-07 |
| Publisher Place | Germany |
| Access Restriction | One Nation One Subscription (ONOS) |
| Content Type | Text |
| Resource Type | Article |
| Subject | Chemistry Nanoscience and Nanotechnology Medicine Biomaterials Engineering Biotechnology |
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