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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Xu, Yang Chen, Ligang Wang, Hui Zhang, Xiaopan Zeng, Qinglei Xu, Haoyan Sun, Lei Zhao, Qi Ding, Lan |
| Description | Country affiliation: China Author Affiliation: Xu Y ( College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, China.) |
| Abstract | In the work, magnetic strong cation exchange (MSCX) resins were prepared using hydrophobic Fe(3)O(4) magnetite as the magnetically susceptible component, styrene and divinylbenzene as polymeric matrix components, acetyl sulfonate as the sulfonation agent. The resins were successfully applied to the extraction of melamine (MEL) from egg samples. The extraction procedure was carried out in a single step by blending and stirring the sample, extraction solvent and the magnetic resins. The MEL was extracted from the sample matrix then adsorbed onto the resins directly through ion-exchange interaction. When the extraction was completed, the resins with adsorbed analyte were easily separated from the sample matrix by applying an appropriate magnetic field. Main factors affecting the extraction of MEL such as the amount of MSCX resins, extraction time, washing and eluting conditions were optimized. The MEL eluted from the resins was determined by liquid chromatography-tandem mass spectrometry. The linearity of quantification obtained by analyzing matrix-matched standards is in the range of 10-1000 ng g(-1). The limit of detection and quantification obtained are 2.6 and 8.8 ng g(-1), respectively. The relative standard deviations of intra- and inter-day ranging from 1.6% to 6.5% and from 2.1% to 7.2% are obtained. The recoveries of MEL are in the range of 77.2-99.3%. The proposed method was successfully applied to determine MEL in eggs obtained from different local markets. MEL was detectable with the contents of 43.5 and 234.1 ng g(-1) in two samples. |
| File Format | HTM / HTML |
| ISSN | 00032670 |
| Issue Number | 1 |
| Journal | Analytica Chimica Acta |
| Volume Number | 661 |
| e-ISSN | 18734324 |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2010-02-19 |
| Publisher Place | Netherlands |
| Access Restriction | One Nation One Subscription (ONOS) |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Environmental Chemistry Analytical Chemistry Biochemistry |
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