NDLI: Preparation of titanium diboride TiB2 by spark plasma sintering at slow heating rate

Content Provider	Taylor & Francis Online
Author	Grin, Yuri Schmidt, Jürgen Burkhardt, Ulrich Boehling, Marian
Abstract	A systematic study of the spark plasma sintering of TiB2 starting from mixture of elemental powders was performed to investigate the temperature distribution between pressing tool and sinter body. The reaction mechanism and time-dependant evolution of the sintering behavior are established. The simultaneous application of pulsed high dc current and load leads to a microstructure with needle-shaped grains. Electron backscattering diffraction analyses show the preferred orientation of small crystallites parallel to the pressing direction.
Starting Page	376
Ending Page	382
Page Count	7
File Format	PDF HTM / HTML
ISSN	14686996 18785514
DOI	10.1016/j.stam.2007.06.009
Journal	Science and Technology of Advanced Materials
Volume Number	8
Issue Number	5
Language	English
Publisher	Taylor & Francis
Publisher Date	2007-08-16
Access Restriction	Open
Subject Keyword	Spark plasma sintering Titanium diboride Microstructure
Content Type	Text
Resource Type	Article
Subject	Materials Science

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Preparation of titanium diboride TiB2 by spark plasma sintering at slow heating rate