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Chemical Research in Chinese Universities : Volume 33

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Efficient synthesis of beraprost sodium

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Efficient synthesis of beraprost sodium

Content Provider	Springer Nature Link
Author	Wang, Yue Hou, Dalong Zhang, Baozhen Lü, Haoze Wang, Ensi
Copyright Year	2016
Abstract	An efficient and straightforward synthesis of beraprost sodium has been developed with dicyclopentadiene as a starting material, a one-pot reaction product 5 as key intermediate and the Prins reaction and the Horner-Wadsworth-Emmons reaction as key steps. The structures of key intermediate and target compound were confirmed by $^{1}$H NMR, $^{13}$C NMR and MS. The purity of beraprost sodium identified by high performance liquid chromatography(HPLC) was identical to that of Japanese Pharmacopoeia(16$^{th}$). This development will be used for the industrial synthesis of beraprost sodium.
Starting Page	581
Ending Page	585
Page Count	5
File Format	PDF
ISSN	10059040
Journal	Chemical Research in Chinese Universities
Volume Number	32
Issue Number	4
e-ISSN	22103171
Language	English
Publisher	Jilin University and The Editorial Department of Chemical Research in Chinese Universities
Publisher Date	2016-07-08
Publisher Place	Changchun
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Chemistry/Food Science Analytical Chemistry Horner-Wadsworth-Emmons reaction Physical Chemistry Inorganic Chemistry Prins reaction Beraprost sodium One-pot reaction Organic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry Education

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