NDLI: Highly sensitive simultaneous quantification of buprenorphine and norbuprenorphine in human plasma by magnetic solid-phase extraction based on PpPDA/Fe$_{3}$O$_{4}$ nanocomposite and high-performance liquid chromatography

Please wait, while we are loading the content...

Journal of the Iranian Chemical Society : Volume 15

Journal of the Iranian Chemical Society : Volume 15, Issue 3, March 2018

Syntheses, crystal structures and biological activities of two new drum-shaped organotin(IV) carboxylate complexes with 2-(4-alkylbenzoyl)benzoic acid (alkyl = methyl or ethyl)

Synthesis of a new magnetic nano-island titania photocatalyst and investigation of its photocatalytic activity

Immobilization of a palladium(II) bis(imidazolium) complex onto graphene oxide by noncovalent interactions: an efficient and recyclable catalyst for Suzuki–Miyaura reaction

Synthesis and characterization of hollow gold nanoparticles by recovery of gold from secondary resources

Study of urease inhibitory activity by medicinal plants extract based on new catalyst for Berthelot reaction and Taguchi experimental design

Exploring the interaction between “site-markers, aspirin and esterase-like activity” ternary systems on the human serum albumin: direct evidence for modulation of catalytic activity of the protein in different inhibition modes

Highly sensitive simultaneous quantification of buprenorphine and norbuprenorphine in human plasma by magnetic solid-phase extraction based on PpPDA/Fe$_{3}$O$_{4}$ nanocomposite and high-performance liquid chromatography

Multivariate investigation of interaction between porphyrin ligands and human telomeric DNA

Aptamer-based sensor for diclofenac quantification using carbon nanotubes and graphene oxide decorated with magnetic nanomaterials

Nanoporous gold electrode prepared from gold compact disk as the anode for the microbial fuel cell

WS$_{2}$ grafted on silicon and nano-silicon particles etched: a high-performance electrocatalyst for hydrogen evolution reaction

Virtual screening of some heterocyclic structures toward novel antibacterial agents

β-Chloro-α,β-unsaturated carbonyls as convenient precursors of highly substituted benzenes

Substituted group-directed assembly of six coordination compounds based on pyrazole bifunctional ligands

Synthesis and characterization of MCM-41@XA@Ni(II) as versatile and heterogeneous catalyst for efficient oxidation of sulfides and acetylation of alcohols under solvent-free conditions

L-phenyl alanine-attached Fe$_{3}$O$_{4}$@SiO$_{2}$ nanoparticles as an efficient catalyst for the synthesis of chromenes

A convenient approach for the synthesis of various derivatives of pyrazolo[1,2-b]phthalazinediones in the presence of an efficient supported basic ionic liquid at ambient temperature and solvent-free media

Exploiting a combined computational/experimental sorbent-injection vortex-assisted dispersive microsolid-phase extraction for chromatographic determination of priority phenolic pollutants in water samples

Synthesis, characterization, cytotoxicity, DNA binding and computational studies of an anionic palladium(II) complex derived from 8-hydroxyquinoline and 1,1-cyclobutanedicarboxylate

A validated chiral LC method for the enantiomeric separation of AT13148 on polysaccharide-based chiral stationary phase

Electrochemical sensing of trifluralin in water by fluconazole-immobilized Fe$_{3}$O$_{4}$/SiO$_{2}$ nanomagnetic core–shell linked to carbon nanotube modified glassy carbon electrode; an experimental and theoretical modeling

Efficient removal of anionic dyes from aqueous media using newly in situ synthesized triazine-based nitrogen-rich network-modified magnetic nanoparticles

The effective removal of mercury ions (Hg$^{2+}$) from water using cadmium sulfide nanoparticles doped in polycaprolactam nanofibers: kinetic and equilibrium studies

Journal of the Iranian Chemical Society : Volume 15, Issue 2, February 2018

Journal of the Iranian Chemical Society : Volume 15, Issue 1, January 2018

Journal of the Iranian Chemical Society : Volume 14

Journal of the Iranian Chemical Society : Volume 13

Journal of the Iranian Chemical Society : Volume 12

Journal of the Iranian Chemical Society : Volume 11

Journal of the Iranian Chemical Society : Volume 10

Journal of the Iranian Chemical Society : Volume 9

Journal of the Iranian Chemical Society : Volume 8

Journal of the Iranian Chemical Society : Volume 7

Journal of the Iranian Chemical Society : Volume 6

Journal of the Iranian Chemical Society : Volume 5

Journal of the Iranian Chemical Society : Volume 4

Journal of the Iranian Chemical Society : Volume 3

Journal of the Iranian Chemical Society : Volume 2

Journal of the Iranian Chemical Society : Volume 1

Highly sensitive simultaneous quantification of buprenorphine and norbuprenorphine in human plasma by magnetic solid-phase extraction based on PpPDA/Fe$_{3}$O$_{4}$ nanocomposite and high-performance liquid chromatography

Content Provider	Springer Nature Link
Author	Madrakian, Tayyebeh Afkhami, Abbas Gomar, Fatemeh
Copyright Year	2017
Abstract	A rapid and sensitive method based on magnetic solid-phase extraction coupled to high-performance liquid chromatography with ultraviolet detection was developed for the simultaneous determination of buprenorphine (BPN) and its major metabolite, norbuprenorphine (N-BPN), in human plasma samples. Poly (para-phenylenediamine)-modified Fe$_{3}$O$_{4}$ nanoparticles (PpPDA/Fe$_{3}$O$_{4}$) were synthesized and used as a magnetic adsorbent for the extraction and preconcentration of BPN and N-BPN in biological samples. The synthesized nanocomposites were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, field emission scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy and vibrating sample magnetometery. An isocratic separation was achieved on a Nova-Pak C18 reversed-phase column using a mobile phase consisting phosphate buffer (pH 3.4) and acetonitrile (50:50, v/v) at a flow rate of 1.0 mL min$^{−1}$. The detection was conducted at 280 nm. Under the optimum conditions, the calibration curves for BPN and N-BPN were linear in the ranges 3.0–150.0 and 1.0–120.0 ng mL$^{−1}$, respectively. The sensitivity was also high with limit of detection of 0.8 and 0.3 ng mL$^{−1}$ for BPN and N-BPN in plasma, respectively. The method was successfully applied to the extraction and determination of BPN and N-BPN in human plasma samples with an average recovery of 98.10 and 96.41%, respectively.
Starting Page	575
Ending Page	585
Page Count	11
File Format	PDF
ISSN	1735207X
Journal	Journal of the Iranian Chemical Society
Volume Number	15
Issue Number	3
e-ISSN	17352428
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2017-12-05
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Analytical Chemistry Buprenorphine Magnetic solid-phase extraction Fe$_{3}$O$_{4}$ nanoparticles Physical Chemistry Poly (para-phenylenediamine) Norbuprenorphine Biochemistry Inorganic Chemistry High-performance liquid chromatography Organic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Fe$_{3}$O$_{4}$@ionic liquid-β-cyclodextrin polymer magnetic solid phase extraction coupled with HPLC for the separation/analysis of congo red

Automated Magnetic Solid-Phase Extraction for Synthetic Food Colorant Determination

graphene / Fe 3 O 4-based magnetic solid phase extraction coupled with high performance liquid chromatography for determination of carvedilol in human blood plasma

Simultaneous quantification of buprenorphine, norbuprenorphine, buprenorphine glucuronide, and norbuprenorphine glucuronide in human placenta by liquid chromatography mass spectrometry

Amino-functionalized Fe$_{3}$O$_{4}$–graphene oxide nanocomposite as magnetic solid-phase extraction adsorbent combined with flame atomic absorption spectrometry for copper analysis in food samples

A magnetic metal/polymer nanocomposite material based on poly(diphenylamine) and Fe$_{3}$O$_{4}$ nanoparticles

Magnetic solid-phase extraction based on Fe 3 O 4 nanoparticles 1 retrieval of chitosan for the determination of flavonoids in biological 2 samples coupled with high performance liquid chromatography

Magnetic solid-phase extraction of imatinib and doxorubicin as cytostatic drugs by Fe$_{3}$O$_{4}$/graphene oxide nanocomposite

Magnetic Solid Phase Extraction of Triazine Herbicides from Environmental Aquatic Media using Polyaniline / Fe 3 O 4 Nanocomposite

Highly sensitive simultaneous quantification of buprenorphine and norbuprenorphine in human plasma by magnetic solid-phase extraction based on PpPDA/Fe$_{3}$O$_{4}$ nanocomposite and high-performance liquid chromatography

Similar Documents

Fe$_{3}$O$_{4}$@ionic liquid-β-cyclodextrin polymer magnetic solid phase extraction coupled with HPLC for the separation/analysis of congo red

Automated Magnetic Solid-Phase Extraction for Synthetic Food Colorant Determination

graphene / Fe 3 O 4-based magnetic solid phase extraction coupled with high performance liquid chromatography for determination of carvedilol in human blood plasma

Simultaneous quantification of buprenorphine, norbuprenorphine, buprenorphine glucuronide, and norbuprenorphine glucuronide in human placenta by liquid chromatography mass spectrometry

Amino-functionalized Fe$_{3}$O$_{4}$–graphene oxide nanocomposite as magnetic solid-phase extraction adsorbent combined with flame atomic absorption spectrometry for copper analysis in food samples

A magnetic metal/polymer nanocomposite material based on poly(diphenylamine) and Fe$_{3}$O$_{4}$ nanoparticles

Magnetic solid-phase extraction based on Fe 3 O 4 nanoparticles 1 retrieval of chitosan for the determination of flavonoids in biological 2 samples coupled with high performance liquid chromatography

Magnetic solid-phase extraction of imatinib and doxorubicin as cytostatic drugs by Fe$_{3}$O$_{4}$/graphene oxide nanocomposite

Magnetic Solid Phase Extraction of Triazine Herbicides from Environmental Aquatic Media using Polyaniline / Fe 3 O 4 Nanocomposite

Highly sensitive simultaneous quantification of buprenorphine and norbuprenorphine in human plasma by magnetic solid-phase extraction based on PpPDA/Fe$_{3}$O$_{4}$ nanocomposite and high-performance liquid chromatography