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Synthesis and characterization of chitosan coating of NiFe$_{2}$O$_{4}$ nanoparticles for biomedical applications

Content Provider	Springer Nature Link
Author	Ramezani, Saeid Sadrnezhaad, Sayed Khatiboleslam Ghazitabar, Arash
Copyright Year	2016
Abstract	Nickel ferrite nanoparticle is a soft magnetic material whose appealing properties as well as various technical applications have rendered it as one of the most attractive class of materials; its technical applications range from its utility as a sensor and catalyst to its utility in biomedical processes. The present paper focuses first on the synthesis of NiFe$_{2}$O$_{4}$ nanoparticles through co-precipitation method resulting in calcined nanoparticles that were achieved at different times and at a constant temperature (773 k). Afterward, they were dispersed in water that was mixed by chitosan. Chitosan was bonded on the surface of nanoparticles by controlling the pH of media. In order to assess the structural and magnetic properties of nanoparticles, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and vibrating sample magnetometer (VSM) analyses were conducted at room temperature. As per the results of XRD analysis, the pure NiFe$_{2}$O$_{4}$ was synthesized. Additionally, nanoparticles grew in size by extending the calcination process duration. TEM micrographs were used to determine the size and shape of particle; the obtained results indicate that the particle size was in a range of 17–30 nm and of a circular shape. The proper chitosan covering was also indicated by FTIR results. The VSM analysis also revealed that the saturated magnetization of NiFe$_{2}$O$_{4}$ nanoparticles stood in a range of 29 emu/g and 45 Q$_{e}$. A stable maximum temperature ranging from 30 to 42 was successfully achieved within 10 min. Also, a specific absorption rate of up to 8.4 W/g was achieved. The study results revealed that the SAR parameter of the coated nickel ferrite nanoparticle is more than that of pure nickel ferrite or cobalt ferrite nanoparticles.
Starting Page	2069
Ending Page	2076
Page Count	8
File Format	PDF
ISSN	1735207X
Journal	Journal of the Iranian Chemical Society
Volume Number	13
Issue Number	11
e-ISSN	17352428
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2016-06-27
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Chitosan biopolymer Analytical Chemistry Physical Chemistry Nickel ferrite nanoparticles SAR parameter Biochemistry Inorganic Chemistry Hyperthermia Organic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry

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