NDLI: Microstructural Analysis and Sintering of Precipitated Silver Chloride Films

Content Provider	Springer Nature Link
Author	Shih, Cheng Chih Lin, C. B.
Copyright Year	2016
Abstract	Silver chloride thin film with high specific surface area was synthesized through heterogeneous precipitation reaction by adding sodium chloride solution on top of frozen silver nitrate solution. The bottom surface (contact with frozen silver nitrate solution) morphology of the silver chloride film comprises numerous porous stick structures. The top surface (contact with sodium chloride solution) consists of equiaxed grains, and columnar grains are observed in the cross section. The effects of sintering temperature and time on the morphology and grain growth mechanisms of the film are also investigated. The grain growth mechanism belongs to an anomalous diffusion involving case I diffusion and case II diffusion. Interface diffusion occurs only at high sintering temperatures, while diffusion-controlled growth dominates at low sintering temperatures. The activation energy of the interface-controlled growth is 50 kJ/mol, while that of diffusion-controlled growth is 10 kJ/mol.
Starting Page	493
Ending Page	504
Page Count	12
File Format	PDF
ISSN	21929262
Journal	Metallography, Microstructure, and Analysis
Volume Number	5
Issue Number	6
e-ISSN	21929270
Language	English
Publisher	Springer US
Publisher Date	2016-11-10
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Silver chloride films Precipitation Sodium chloride Silver nitrate Morphology Growth mechanisms Metallic Materials Characterization and Evaluation of Materials Structural Materials Surfaces and Interfaces, Thin Films Nanotechnology
Content Type	Text
Resource Type	Article
Subject	Metals and Alloys

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