NDLI: Physical Property Characterization of Pb$^{2+}$-Doped CdS Nanofilms Deposited by Chemical-Bath Deposition at Low Temperature

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Physical Property Characterization of Pb$^{2+}$-Doped CdS Nanofilms Deposited by Chemical-Bath Deposition at Low Temperature

Content Provider	Springer Nature Link
Author	Díaz Reyes, J. Contreras Rascón, J. I. Galván Arellano, M. Arias Cerón, J. S. Gutiérrez Arias, J. E. M. Flores Mena, J. E. Morín Castillo, M. M.
Copyright Year	2016
Abstract	Pb$^{2}$ $^{+}$-doped CdS nanofilms are prepared using the growth technique chemical bath deposition (CBD) under optimum conditions lead acetate at the reservoir temperature of 20 ± 2 °C. The Pb$^{2+}$ molar concentration was in the range 0.0 ≤ x ≤ 0.19.67, which was determined by energy-dispersive X-ray spectroscopy (EDS). The X-ray diffraction results show that the films are of PbS–CdS composites with individual CdS and PbS planes. The X-ray diffraction (XRD) analysis and Raman scattering reveal that CdS-deposited films showed the zincblende (ZB) crystalline phase. The average grain size of the CdS films ranged from 1.21 to 6.67 nm that was determined by the Debye–Scherrer equation from ZB (111) direction, and it was confirmed by high-resolution transmission electron microscopy (HRTEM). Raman scattering shows that the lattice dynamics is characteristic of bimodal behaviour and the multipeaks adjust of the first optical longitudinal mode for the Pb$^{2+}$-doped CdS denotes the Raman shift of the characteristic peak in the range of 305–298 cm$^{−1}$ of the CdS crystals, which is associated with the lead ion incorporation. The films exhibit three direct bandgaps, ~2.44 eV attributed to CdS; the other varies continuously from 1.67 to 1.99 eV and another disappears as Pb$^{2+}$ molar fraction increases.
Starting Page	612
Ending Page	620
Page Count	9
File Format	PDF
ISSN	01039733
Journal	Brazilian Journal of Physics
Volume Number	46
Issue Number	6
e-ISSN	16784448
Language	English
Publisher	Springer US
Publisher Date	2016-08-22
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Chemical bath deposition Semiconductor compounds II–VI CdS:Pb$^{2+}$ Raman spectroscopy X-ray diffraction Transmittance Physics
Content Type	Text
Resource Type	Article
Subject	Physics and Astronomy

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