NDLI: Synthesis and Characterization of Zinc Fluoroborate from Zinc Fluoride and Boron by Mechanochemical Reaction

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Synthesis and Characterization of Zinc Fluoroborate from Zinc Fluoride and Boron by Mechanochemical Reaction

Content Provider	Springer Nature Link
Author	Aydın, Duygu Y. Gürü, Metin Ipek, Dilek Özyürek, Dursun
Copyright Year	2017
Abstract	This paper deals with characterization and synthesis of zinc fluoroborate from zinc fluoride and boron by mechanochemical reaction. Zinc fluoroborate is widely used in high technological areas such as textile, chemical reaction, plating solution, and glass. In this study, zinc fluoroborate has been synthesized via high-energy ball milling method. The effect of reactant mol ratio (B/ $$\hbox {ZnF}_{2})$$ and ball milling period was investigated on the product yield. After completion of the reaction, the product in the reaction mixture (including excess reactant and side products) was purified by the extraction with water. The samples were characterized by FT-IR and $$\hbox {BF}_{4}^{-}$$ ion-selective electrode. SEM and EDX analyses were took place. Decomposition of sample was characterized by TG-DTA. The sample was sintered at 300– $$500\,{^{\circ }}\hbox {C}$$ to compare the data with TG-DTA. The results showed that decomposition of B–F bond started at $$300\,{^{\circ }}\hbox {C}$$ . As a result of these experiments, maximum yield was obtained at 0.8 molar ratio and 3000 min. of mechanochemical reaction duration with the use of ball milling. Eighty-three percentage pure zinc fluoroborate was produced by adding the purification step.
Starting Page	4409
Ending Page	4416
Page Count	8
File Format	PDF
ISSN	2193567X
Journal	Arabian Journal for Science and Engineering
Volume Number	42
Issue Number	10
e-ISSN	21914281
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2017-04-27
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Zinc fluoroborate Mechanochemical reaction Ball milling $$\hbox {ZnF}_{2}$$ Boron Engineering Science, Humanities and Social Sciences, multidisciplinary
Content Type	Text
Resource Type	Article
Subject	Multidisciplinary

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