NDLI: Comparison between inductively coupled plasma and X-ray fluorescence performance for Pb analysis in environmental soil samples

Content Provider	Springer Nature Link
Author	Al Maliki, Ali Al lami, Ahmed Kadhim Hussain, H. M. Al Ansari, Nadhir
Copyright Year	2017
Abstract	Comparison of two conventional analytical techniques such as X-ray fluorescence (XRF) and inductively coupled plasma mass spectrometry (ICP-MS) for measuring Pb concentrations in soil samples was achieved using field and laboratory work. Seventy-three samples were collected from urban areas surrounding the large lead smelter at South Australia, as an indicator of the environment impact of smelter activity. Soil Pb concentrations were determined using hand-held XRF analyser under laboratory conditions. ICP-MS analysis on digested soils (using a microwave-assisted nitric acid digestion-extraction) was applied to validate p-XRF data. The analysis showed that Pb concentrations determined by XRF correlated with high linearity with Pb concentrations determined by ICP-MS measurements (R $^{2}$ = 0.89). Statistical test (t test) was applied to the data of both methods applied without any significant difference between the two techniques. These results indicated that ICP-MS corroborated XRF for Pb soil measurements and suggests that XRF was a reliable and quick alternative to traditional analytical methods in studies of environmental health risk assessment, allowing for much larger sampling regimes in relatively shorter times and could be applied in the field.
Starting Page	1
Ending Page	7
Page Count	7
File Format	PDF
ISSN	18666280
Journal	Environmental Earth Sciences
Volume Number	76
Issue Number	12
e-ISSN	18666299
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2017-06-26
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	ICP-MS Soil Pb contamination XRF Heavy metal Geology Hydrology/Water Resources Geochemistry Environmental Science and Engineering Terrestrial Pollution Biogeosciences
Content Type	Text
Resource Type	Article
Subject	Global and Planetary Change Earth-Surface Processes Soil Science Environmental Chemistry Pollution Geology Water Science and Technology

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