NDLI: Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids

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Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids

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Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids

Content Provider	Springer Nature Link
Author	Fukuda, Yuuki Ando, Yasuhiro
Copyright Year	2011
Abstract	Fatty acid analysis of roughscale sole Clidoderma asperrimum flesh lipids was carried out by gas chromatography. An unidentified peak appeared in the chromatogram in the elution region of ≥C24 fatty acids. After enrichment by solvent partitioning, reversed-phase thin-layer chromatography (TLC), and argentation TLC, the peak component was subjected to structural analyses. The partially hydrogenated products after reaction with hydrazine hydrate gave seven isomers of cis-hexacosenoic acid (26:1). Gas chromatography-mass spectrometry (GC–MS) analyses of their dimethyl disulfide adducts identified the monounsaturates as 5-, 8-, 11-, 14-, 17-, 20-, and 23-26:1. The peak component was assigned to all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3). GC–MS analyses of the 4,4-dimethyloxazoline derivative and methyl ester confirmed this structure. This fatty acid is a rare, very long-chain polyunsaturated fatty acid (VLCPUFA). The concentrations of the acid found in roughscale sole were 0.69 ± 0.34% (N = 5) of total fatty acids in flesh lipids. Roughscale sole appears to be characterized by the occurrence of 26:7n-3, which is lacking in popular sources of methylene-interrupted VLCPUFA, such as vertebrate retina, spermatozoa, and herring.
Starting Page	875
Ending Page	882
Page Count	8
File Format	PDF
ISSN	09199268
Journal	Fisheries Science
Volume Number	77
Issue Number	5
e-ISSN	14442906
Language	English
Publisher	Springer Japan
Publisher Date	2011-07-13
Publisher Place	Japan
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Hexacosaheptaenoic acid Very long-chain polyunsaturated fatty acid Fatty acid Roughscale sole Clidoderma asperrimum GC GC–MS Food Science Freshwater & Marine Ecology Fish & Wildlife Biology & Management
Content Type	Text
Resource Type	Article
Subject	Aquatic Science

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Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids

Morphological and habitat characteristics of settling and newly settled Roughscale Sole Clidoderma asperrimum collected in the coastal waters of northeastern Japan

The first capture of roughscale sole Clidoderma asperrimum in the northwestern part of the Sea of Japan

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Occurrence and distribution of cis-7-icosenoic acid in the lipids of Japanese marine fish, shellfish, and crustaceans

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Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids

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