NDLI: A Simple and Rapid Method for Determination of Patulin in Juice by High Performance Liquid Chromatography Tandem Mass Spectrometry

Content Provider	Springer Nature Link
Author	Yang, Yi Yang, Yunjia Shao, Bing Zhang, Jing
Copyright Year	2017
Abstract	A simple and rapid method was developed for analysis of patulin in juice using ultra performance liquid chromatography coupled with tandem mass spectrometry. The samples were purified by an Oasis MAX 96-Well Plate. Chromatographic separation was performed on an ACQUITY UPLC® HSS T3 column with gradient elution using acetonitrile and water as mobile phase. Analytes was quantified by external calibration curves over the ranges of 0.50–50 μg/L, with correlation coefficients > 0.9986. The LOD and LOQ in juice sample were 0.30 and 1.0 μg/L, respectively. Recoveries of the method (spiked at levels of 1, 5, 25 and 50 μg/L) ranged from 91.6% to 95.7%, while intraday and interday relative standard deviations were 6.87–11.0% and 6.53–11.6%, respectively.
Starting Page	2913
Ending Page	2918
Page Count	6
File Format	PDF
ISSN	19369751
Journal	Food Analytical Methods
Volume Number	10
Issue Number	9
e-ISSN	1936976X
Language	English
Publisher	Springer US
Publisher Date	2017-03-09
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Patulin Juice UPLC-MS/MS Food Science Chemistry/Food Science Microbiology Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Safety Research Safety, Risk, Reliability and Quality Applied Microbiology and Biotechnology Food Science

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A Simple and Rapid Method for Determination of Patulin in Juice by High Performance Liquid Chromatography Tandem Mass Spectrometry