NDLI: Synthesis, characterization and magnetic property of 3D flower-like nickel sulphide nanocrystals through decomposing bis(thiourea) nickel(II) chloride crystals

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Synthesis, characterization and magnetic property of 3D flower-like nickel sulphide nanocrystals through decomposing bis(thiourea) nickel(II) chloride crystals

Content Provider	Springer Nature Link
Author	YIN, PENG FEI SUN, LI LI ZHOU, CHAO SUN, YU HENG HAN, XIANG YU DENG, CHENG RONG
Copyright Year	2015
Abstract	Three-dimensional (3D) flower-like cubic Ni$_{3}$S$_{4}$ nanoplates with single crystalline nature were successfully prepared through decomposing bis(thiourea) nickel(II) chloride crystals (BTNC). The samples were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope, selected area electron diffraction and Raman spectroscopy. Results show that the as-prepared products are pure cubic Ni$_{3}$S$_{4}$ and stable in range of 180–220°C with single crystal nature providing high surface areas, and higher reaction temperature leads to lower surface areas. Typical Raman peaks of the as-synthesized 3D flower-like cubic Ni$_{3}$S$_{4}$ at 200°C are located at 239, 286, 337, 379, 423, 478 and 630 cm$^{−1}$. Magnetization measurement indicates that single crystalline Ni$_{3}$S$_{4}$ nanoplates prepared at 200°C displays antiferromagnetic behaviour.
Starting Page	95
Ending Page	99
Page Count	5
File Format	PDF
ISSN	02504707
Journal	Bulletin of Materials Science
Volume Number	38
Issue Number	1
e-ISSN	09737669
Language	English
Publisher	Springer India
Publisher Date	2015-02-13
Publisher Institution	Indian Academy of Sciences
Publisher Place	India
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Nanocrystal thermal decomposition BTNC nickel sulphide characterization magnetic property. Materials Science Engineering
Content Type	Text
Resource Type	Article
Subject	Mechanics of Materials Materials Science

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