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Phase, microstructure, and oxidation resistance of yttrium silicates coatings prepared by a hydrothermal electrophoretic deposition process for C/C composites

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Phase, microstructure, and oxidation resistance of yttrium silicates coatings prepared by a hydrothermal electrophoretic deposition process for C/C composites

Content Provider	Springer Nature Link
Author	Miao, Liu Jianfeng, Huang Yutao, Zhang Fei, Deng Liyun, Cao Jianpeng, Wu
Copyright Year	2008
Abstract	Oxidation-resistant yttrium silicates coatings for SiC precoated carbon/carbon composites were prepared by a novel hydrothermal electrophoretic deposition process. Sonochemical-synthesized yttrium silicates nanocrystallites, isopropanol, and iodine were respectively used as source materials, solvent, and charging agent during the deposition. Phase compositions, surface and cross-section microstructures of the as-prepared multilayer coatings were characterized by an X-ray diffractometer (XRD) and a scanning electron microscopy (SEM). The influence of deposition temperatures on the phase, microstructure, and oxidation resistance of the multilayer coated C/C composites was particularly investigated. Results show that the as-prepared outer coatings are composed of yttrium silicates crystallites with a main phase of Y$_{2}$Si$_{2}$O$_{7}$ and Y$_{2}$SiO$_{5}$. The thickness and density of the yttrium silicates coatings are improved with the increase of deposition temperature. Compared with SiC coating prepared by pack cementation, the multilayer coatings prepared by pack cementation with a later hydrothermal electrophoretic deposition process exhibit better antioxidation properties. The as-prepared multilayer coatings can effectively protect C/C composites from oxidation at 1773 K in air for 35 h with a weight loss of 0.32 × 10$^{−3}$ g/cm$^{2}$.
Starting Page	531
Ending Page	535
Page Count	5
File Format	PDF
ISSN	15470091
Journal	JCT Research
Volume Number	6
Issue Number	4
e-ISSN	19353804
Language	English
Publisher	Springer US
Publisher Date	2008-07-24
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Carbon/carbon composites Yttrium silicates Hydrothermal electrophoretic deposition Materials Science Industrial Chemistry/Chemical Engineering Polymer Sciences Surfaces and Interfaces, Thin Films Tribology, Corrosion and Coatings
Content Type	Text
Resource Type	Article
Subject	Chemistry Surfaces, Coatings and Films Colloid and Surface Chemistry Surfaces and Interfaces

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