NDLI: Graphite to Graphene via Graphene Oxide: An Overview on Synthesis, Properties, and Applications

Content Provider	Springer Nature Link
Author	Hansora, D. P. Shimpi, N. G. Mishra, S.
Copyright Year	2015
Abstract	This work represents a state-of-the-art technique developed for the preparation of graphene from graphite–metal electrodes by the arc-discharge method carried out in a continuous flow of water. Because of continuous arcing of graphite-metal electrodes, the graphene sheets were observed in water with uniformity and little damage. These nanosheets were subjected to various purification steps such as acid treatment, oxidation, water washing, centrifugation, and drying. The pure graphene sheets were analyzed using Raman spectrophotometry, x-ray diffraction (XRD), field emission-scanning electron microscopy (FE-SEM), and tunneling electron microscopy (TEM). Peaks of Raman spectra were recorded at (1300–1400 cm$^{−1}$) and (1500–1600 cm$^{−1}$) for weak D-band and strong G-band, respectively. The XRD pattern showed 85.6% crystallinity of pure graphite, whereas pure graphene was 66.4% crystalline. TEM and FE-SEM micrographs revealed that graphene sheets were overlapped to each other and layer-by-layer formation was also observed. Beside this research work, we also reviewed recent developments of graphene and related nanomaterials along with their preparations, properties, functionalizations, and potential applications.
Starting Page	2855
Ending Page	2868
Page Count	14
File Format	PDF
ISSN	10474838
Journal	JOM
Volume Number	67
Issue Number	12
e-ISSN	15431851
Language	English
Publisher	Springer US
Publisher Date	2015-07-03
Publisher Institution	The Minerals, Metals & Materials Society (TMS)
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Engineering Chemistry/Food Science Physics Environment Earth Sciences
Content Type	Text
Resource Type	Article
Subject	Engineering Materials Science

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