NDLI: Synthesis of mesoporous silica in acidic condition by solvent evaporation method

Content Provider	Springer Nature Link
Author	Roh, Hyun Seog Chang, Jong San Park, Sang Eon
Copyright Year	1999
Abstract	Both powder-type and film-type mesoporous silica materials have been prepared by using a sol-gel process in highly acidic, solvent-rich and mild conditions by solvent evaporation method. Powder mesoporous silica which has hexagonal arrays was well synthesized within only 10 minutes, and mesoporous film was formed on the glass plate within only several seconds by supramolecular interactions between the silicate species and surfactant-templates. In particular, the synthesis time was very short compared with that of hydrothermal synthesis owing to the solvent evaporation. This method has some characteristics different from the hydrothermal method such as the following. There is no precipitation because particles do not form in the solution before solvent evaporation, bulk powder is rigid, whereas that of hydrothermal synthesis is very soft, and mesoporous materials are synthesized in acidic condition. Solvent evaporation method for the synthesis of mesoporous materials is promising because the method is very simple and time-saving.
Starting Page	331
Ending Page	337
Page Count	7
File Format	PDF
ISSN	02561115
Journal	Korean Journal of Chemical Engineering
Volume Number	16
Issue Number	3
e-ISSN	19757220
Language	English
Publisher	Springer-Verlag
Publisher Date	1999-01-01
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Mesoporous Silica Solvent Evaporation Method Supramolecular Interactions Acidic Condition Industrial Chemistry/Chemical Engineering Catalysis Materials Science Biotechnology
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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