NDLI: Preparation of spherical macroporous silica in an aerosol phase

Content Provider	Springer Nature Link
Author	Ahn, Ki Woong Rah, Hana Kim, Sun Geon
Copyright Year	2012
Abstract	Macroporous silica (MS) and macro/mesoporous silica (MMS) were prepared by spray drying a polystyrene (PS) latex sol containing a silica source, followed by calcination. As a silica source, 3-aminopropyl triethoxysilane (APS) was used for MS while either silica sol (SS) or tetraethoxyothosilicate using P123 templating (P123-TEOS) was used for MMS. Spray drying and calcination could also take place in a once-through aerosol reactor. The transformation of the silicon alkoxides to silica and decomposition of PS occurred at similar temperatures. Therefore, for APS-originated MS, the metal additives such as silver and nickel were required to accelerate the former. In addition, the nickel was well dispersed in the silica matrix during calcination even at 800 °C, in turn to thermally stabilize the porous structures. The wall-preforming additives were unnecessary for PS/SS and PS/P123-TEOS, since the SS drying and P123 templating, respectively, took place at lower temperature than PS decomposition. The porosities of all the porous silica prepared ranged from 0.54 to 0.57, which were close to the volume fraction of PS in the PS-alkoxides mixture solidified right after spray drying.
Starting Page	1444
Ending Page	1452
Page Count	9
File Format	PDF
ISSN	02561115
Journal	Korean Journal of Chemical Engineering
Volume Number	29
Issue Number	10
e-ISSN	19757220
Language	English
Publisher	Springer US
Publisher Date	2012-03-16
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Industrial Chemistry/Chemical Engineering Materials Science Biotechnology Catalysis
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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