NDLI: A study on the synthesis of acrylic composite particles and investigation of their characterization

Content Provider	Springer Nature Link
Author	Lee, Sun Ryong Seul, Soo Duk
Copyright Year	2002
Abstract	Core-shell latexes were synthesized by sequential emulsion polymerization of methyl methacrylate (MMA), styrene (St), and ethyl acrylate (EA) in the presence of anionic surfactant, and the characteristics of these latexes were evaluated. The core latex had to be synthesized carefully to avoid the formation of secondary particles. The sequential polymerization method adopted for this synthesis took advantage of stabilizing particles grown during shell polymerization. In core-shell latex polymerization, to suppress the generation of new particles and to minimize the gelation during the shell polymerization, the amount of surfactant (Sodium dodecyl benzene sulfonate: SDBS) should be reduced to the minimum, 0.01 wt% and 0.02 wt% of SDBS to amount of monomer, respectively, when the Polymethyl methacrylate (PMMA) and Polystyrene (PSt) core latexes are prepared. In addition, the monomer pre-emulsion method is better than monomer-add method. The core-shell structure for composite latex synthesized was demonstrated by Particle Size Analysis (PSA), Differential Scanning Calorimeter (DSC), Transmission Electron Microscope (TEM), formability of film, and hydrolysis under NaOH solution.
Starting Page	318
Ending Page	323
Page Count	6
File Format	PDF
ISSN	02561115
Journal	Korean Journal of Chemical Engineering
Volume Number	19
Issue Number	2
e-ISSN	19757220
Language	English
Publisher	Springer-Verlag
Publisher Date	2002-01-01
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Core-shell Latex Polymethyl Methacrylate Polystyrene Sequential Emulsion Polymerization Industrial Chemistry/Chemical Engineering Catalysis Materials Science Biotechnology
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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