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Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquid chromatography-tandem mass spectrometry

Content Provider	Springer Nature Link
Author	Wei, Yimei Zhang, Yuan Xu, Jian Guo, Changsheng Li, Lei Fan, Wenhong
Copyright Year	2013
Abstract	Precise and sensitive methods for the simultaneous determination of different classes of antibiotics, including sulphonamides, fluoroquinolones, macrolides, tetracyclines, and trimethoprim in surface water, sediments, and fish muscles were developed. In water samples, drugs were extracted with solid-phase extraction (SPE) by passing 1000 mL of water through hydrophilic lipophilic balanced (HLB) SPE cartridges. Sediment samples were solvent-extracted, followed by tandem SPE (strong anion exchange (SAX) + HLB) clean-ups. Fish muscles were extracted by a mixture of acetonitrile and citric buffer (80:20, v/v) solution, and cleaned by SPE. Liquid chromatography-tandem mass spectrometry (LC-MS/MS) with multiple reaction monitoring (MRM) detection was employed to quantify all compounds. The recoveries for the antibiotics in the spiked water, sediment, and fish samples were 60.2%–95.8%, 48.1%–105.3%, and 59.8%–103.4%, respectively. The methods were applied to samples taken from Dianchi Lake, China. It showed that concentrations of the detected antibiotics ranged from limits of quantification (LOQ) to 713.6 ng·L$^{−1}$ (ofloxacin) in surface water and from less than LOQ to 344.8 μg·kg$^{−1}$ (sulphamethoxazole) in sediments. The number of detected antibiotics and the overall antibiotic concentrations were higher in the urban area than the rural area, indicating the probable role of livestock and human activities as important sources of antibiotic contamination. In fish muscles, the concentration of norfloxacin was the highest (up to 38.5 μg·kg$^{−1}$), but tetracyclines and macrolides were relatively low. Results showed that the methods were rapid and sensitive, and capable of determining several classes of antibiotics from each of the water, sediment, and fish matrices in a single run.
Starting Page	357
Ending Page	371
Page Count	15
File Format	PDF
ISSN	20952201
Journal	Frontiers of Environmental Science & Engineering in China
Volume Number	8
Issue Number	3
e-ISSN	2095221X
Language	English
Publisher	Higher Education Press
Publisher Date	2013-10-14
Publisher Institution	Chinese Universities
Publisher Place	Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	antibiotics liquid chromatography-tandem mass spectrometry (LC-MS/MS) water sediment fish muscle Environment
Content Type	Text
Resource Type	Article
Subject	Environmental Science

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