NDLI: Effect of sintering additives on properties of Si$_{3}$N$_{4}$-BN composites fabricated via die pressing and precursor infiltration and pyrolysis route

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Effect of sintering additives on properties of Si$_{3}$N$_{4}$-BN composites fabricated via die pressing and precursor infiltration and pyrolysis route

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Effect of sintering additives on properties of Si$_{3}$N$_{4}$-BN composites fabricated via die pressing and precursor infiltration and pyrolysis route

Content Provider	Springer Nature Link
Author	Liu, Kun Zhang, Changrui Li, Bin Wang, Siqing Cao, Feng
Copyright Year	2014
Abstract	The Si$_{3}$N$_{4}$-BN composites have been prepared via die pressing and precursor infiltration and pyrolysis route using borazine as precursor, and the effect of sintering additives on properties of the composites has been investigated. After sintering additives are adopted, the α to β phase transition of Si$_{3}$N$_{4}$ and the mechanical properties of the composites at both room temperature and high temperature are all increased with small extent. When using Y$_{2}$O$_{3}$+Al$_{2}$O$_{3}$ as additives, the phase transition of Si$_{3}$N$_{4}$ and the mechanical properties of the composites have better results. The β-Si$_{3}$N$_{4}$ content is 17.47%. The flexural strength, elastic modulus and fracture toughness of the composites are 188.74 MPa, 84.34 GPa and 2.96 MPa·m$^{1/2}$, respectively. After exposed at 1 000 °C in the air for 15 min, the flexural strength of the composites is 154.62 MPa with a residual ratio of 81.92%. The elongated β-Si$_{3}$N$_{4}$ grains appear in all composites with different sintering additives. Relatively more rod like β-Si$_{3}$N$_{4}$ grains can be observed in composites with Y$_{2}$O$^{3+}$Al$_{2}$O$_{3}$ as additives, making it to possess better mechanical properties.
Starting Page	891
Ending Page	894
Page Count	4
File Format	PDF
ISSN	10002413
Journal	Journal of Wuhan University of Technology-Mater. Sci. Ed.
Volume Number	29
Issue Number	5
e-ISSN	19930437
Language	English
Publisher	Wuhan University of Technology
Publisher Date	2014-10-04
Publisher Place	Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	silicon nitride boron nitride borazine composites sintering additives Materials Science
Content Type	Text
Resource Type	Article
Subject	Materials Science

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Effect of sintering additives on properties of Si$_{3}$N$_{4}$-BN composites fabricated via die pressing and precursor infiltration and pyrolysis route

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