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A new method of preparing alkanethiol-protected gold nanoparticals

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A new method of preparing alkanethiol-protected gold nanoparticals

Content Provider	Springer Nature Link
Author	Xiao ya, Hu Qin, Xu Rong, Guo
Copyright Year	2003
Abstract	In a new two-phase system (tetrahydrofuran/saturated NaCl aqueous solution) monolayer protected clusters (MPCs) were prepared. The AuCl 4 − anion in saturated electrolyte aqueous solution was transferred into the organic phase of tetrahydrofuran by tetra-n-butylammonium bromide ((C$_{4}$H$_{9}$)$_{4}$NBr) and was reduced quickly by sodium borohydride in the presence of alkanethiol. The functionalized MPCs were characterized by solubility, transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), energy-dispersive X-ray (EDX) analysis and UV-vis spectroscopy. Electrochemical measurements of MPCs in CH$_{2}$ Cl$_{2}$ exhibited 7 pairs of reversible voltammetric waves within the potential range of −1.0 to 1.0V (vs Ag/AgCl), which was ascribed to the quantized capacitance charging of nanoparticle double layers. All the results show that the new preparing method is feasible.
Starting Page	1
Ending Page	5
Page Count	5
File Format	PDF
ISSN	10002413
Journal	Journal of Wuhan University of Technology-Mater. Sci. Ed.
Volume Number	18
Issue Number	4
e-ISSN	19930437
Language	English
Publisher	Wuhan University of Technology
Publisher Date	2003-01-01
Publisher Place	Wuhan
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	chemical preparation monolayer protected cluster quantized charging Materials Science
Content Type	Text
Resource Type	Article
Subject	Materials Science

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Quantized capacitance charging of monolayer-protected Au clusters

Electrochemical characterization of self-assembled monolayers on gold substrates derived from thermal decomposition of monolayer-protected cluster films

Electrochemical Quantized Capacitance Charging of Surface Ensembles of Gold Nanoparticles

Investigation of interparticle interactions of larger (4.63 nm) monolayer protected gold clusters during quantized double layer charging.

Preparation of Gold Nanoparticles Protected by a Cubic Silsesquioxane and Their Monolayer Formation on a Glass Substrate

Chemical Physics Letters 338 �2001) 33±36 www.elsevier.nl/locate/cplett Oxidation of alkanethiol monolayers on gold cluster surfaces (2001)

Size-dependent quantized double layer charging of monolayer-protected silver nanoparticles

Electrocatalysis by Polyoxometalate-Protected Gold Nanoparticles

Preparation and comparison between different thiol-protected Au nanoparticles

A new method of preparing alkanethiol-protected gold nanoparticals

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