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  1. Journal of Wuhan University of Technology-Mater. Sci. Ed.
  2. Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30
  3. Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 4, August 2015
  4. Study on the pyrolysis behavior of polycarbosilane
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Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 32
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 31
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 6, December 2015
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 5, October 2015
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 4, August 2015
Synthesis and performance of LiFe$_{ x }$Mn$_{1−x }$PO$_{4}$/C as cathode material for lithium ion batteries
Structural and optical properties of Ce$^{3+}$, Yb$^{3+}$ Co-doped YAG films by pulsed laser deposition
Preparation and magnetic properties of Cu-Ni core-shell nanowires in ion-track templates
Hydrogenation/dehydrogenation performances of the MgH$_{2}$-WS$_{2}$ composites
The influences of controlling sintering mechanism on electrical properties of multilayer PTCR chip
Study on the pyrolysis behavior of polycarbosilane
Effects of heating processing on microstructure and magnetic properties of Mn-Zn ferrites prepared via chemical co-precipitation
Effects of processing conditions on the properties of epoxy resin microcapsule
Rheological evaluation of polymer modified asphalt binders
Impact of freeze-thaw cycles on compressive characteristics of asphalt mixture in cold regions
In-situ preparation of TiB$_{2}$-TiB-Ti functionally graded materials by improved sintering process
Near infrared luminescence of bismuth-doped MO-B$_{2}$O$_{3}$ (M=Ca, Sr, Ba) glasses
Preparation of MgF$_{2}$ translucent ceramic by hot pressing sintering
Preparation and piezoelectric properties of CuO-added (Ag$_{0.75}$Li$_{0.1}$Na$_{0.1}$K$_{0.05}$)NbO$_{3}$ lead-free ceramics
Preparation of nano-sized zirconium carbide powders through a novel active dilution self-propagating high temperature synthesis method
Spatial distribution of the increased porosity of cement paste due to calcium leaching
Effect of hydration aging and water binder ratio on microstructure and mechanical properties of sprayed concrete
Impact resistance of reactive powder concrete
Chemical composition and microstructure of hydration products of hardened white portland cement pastes containing admixtures
Effect of Nano-TiO$_{2}$ addition on the hydration and hardening process of sulphoaluminate cement
Investigation on the thermo-dynamics of alkali-activated carbonatite
Leaching behavior and mechanism of cement solidified heavy metal Pb in acid medium
Preparation for retarding and high early strength concrete
Tensile strength and oxide analysis of carbon steel in concrete exposed in atmospheric environment for 53 years
Relationship between heat treatment and corrosion behavior of Mg-15Y alloy
Effect of laser remelting on the microstructure and corrosion resistance of plasma sprayed Fe-based coating
Cyclic oxidation resistance of In718 superalloy treated by laser peening
Self-healing performance of composite coatings prepared by phosphating and cerium nitrate post-sealing
Dynamic observation of bainite transformation in a Fe-C-Mn-Si superbainite steel
Characterization and properties of duplex a-C:H/MAO coatings on magnesium alloy using combined microarc oxidation and hybrid magnetron sputtering
Microstructure and mechanical properties of AerMet 100 ultra-high strength steel joints by laser welding
Nanoindentation mechanical properties and structural biomimetic models of three species of insects wings
Electrospinning and rheological behavior of poly (vinyl alcohol)/collagen blended solutions
Effect of a nerve graft substitute single-walled carbon nanotubes on rat pheochromocytoma cells
Synthesis and evaluation of novel chitosan derivatives for gene delivery
Preparation and action mechanism of inclusion complex of β-cyclodextrin and sulfurized isobutylene as additives in solution of polyethylene glycol-600
Magnetic property of a spin-5/2 trigonal prismatic as a model for a molecule-based compound Cs$_{4}$Na$_{7}$[Fe$_{6}$(OH)$_{3}$(A-α-GeW$_{9}$O$_{34}$(OH)$_{3}$)$_{2}$]・30H$_{2}$O
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 3, June 2015
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 2, April 2015
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 30, Issue 1, February 2015
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 29
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 28
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 27
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 26
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 25
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 24
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 23
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 22
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 21
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 20
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 19
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 18
Journal of Wuhan University of Technology-Mater. Sci. Ed. : Volume 17

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Study on the pyrolysis behavior of polycarbosilane

Content Provider Springer Nature Link
Author Chen, Wenyi Zhou, Jian
Copyright Year 2015
Abstract The pyrolysis behavior of polycarbosilane (PCS) and chemical reaction mechanism during the pyrolysis process were studied by thermogravimetric-mass spectrometry (TG-MS) combined with X-ray diffraction and infrared spectroscopic analysis methods. The experimental results indicate that the main gas phase products generated during pyrolysis of PCS in nitrogen atmosphere include H$_{2}$, -CH$_{3}$ and CH$_{4}$. The heating rate has a large effect on the pyrolysis process of PCS, the lower heating rate releases more small molecule gases and gets bigger rate of pyrolysis mass loss, demonstrating that the lower heating rate is beneficial to fully pyrolysis of PCS and obtain ceramics products with better microstructure.
Starting Page 679
Ending Page 683
Page Count 5
File Format PDF
ISSN 10002413
Journal Journal of Wuhan University of Technology-Mater. Sci. Ed.
Volume Number 30
Issue Number 4
e-ISSN 19930437
Language English
Publisher Wuhan University of Technology
Publisher Date 2015-07-30
Publisher Place Wuhan
Access Restriction One Nation One Subscription (ONOS)
Subject Keyword polycarbosilane pyrolysis behavior thermogravimetric-mass spectrometry heating rate mass loss Materials Science
Content Type Text
Resource Type Article
Subject Materials Science
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