NDLI: Synthesis and electrical properties of Ln$_{2}$CuO$_{4+}$ $_{ δ }$ (Ln: Nd or La) mixed conductor sputter deposited coatings

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Synthesis and electrical properties of Ln$_{2}$CuO$_{4+}$ $_{ δ }$ (Ln: Nd or La) mixed conductor sputter deposited coatings

Content Provider	Springer Nature Link
Author	Briois, P. Oliveira, J. C. Lapostolle, F. Perry, F. Billard, A. Cavaleiro, A.
Copyright Year	2007
Abstract	Nd$_{2}$CuO$_{4}$ and La$_{2}$CuO$_{4}$ are potential candidates as cathode material for intermediate temperature-solid oxide fuel cells. Nd–Cu and La–Cu oxides were co-sputtered on rotating substrates from metallic La, Nd and Cu targets in the presence of a reactive argon–oxygen gas mixture. Structural and chemical features of these films have been determined by X-ray diffraction and energy-dispersive spectroscopy. Their electrical resistivity was measured using the four-point probe method. As-deposited Nd–Cu based coatings are amorphous and, after annealing, crystallise in K$_{2}$NiF$_{4+}$ $_{ δ }$ -type structure for Nd/Cu atomic ratio of 2, with more or less Nd$_{2}$O$_{3}$ or CuO, depending on whether Nd or Cu is in excess, respectively. As-deposited La–Cu based coatings are also amorphous and crystallise in La$_{2}$CuO$_{4}$ for La/Cu >2 or in LaCuO$_{3±δ }$ perovskite-type structure when Cu is in excess. The electrical measurements show a clear relation between resistivity and structure of the coatings. After annealing, crystallised neodymium-based coatings show higher resistivity than lanthanum-based ones. Finally, LaCuO$_{3±δ }$ exhibit higher resistivity than La$_{2}$CuO$_{4}$.
Starting Page	455
Ending Page	461
Page Count	7
File Format	PDF
ISSN	09477047
Journal	Ionics
Volume Number	14
Issue Number	5
e-ISSN	18620760
Language	English
Publisher	Springer-Verlag
Publisher Date	2008-01-14
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Magnetron sputtering La$_{2}$CuO$_{4}$ LaCuO$_{3}$ Nd$_{2}$CuO$_{4}$ Cathode material IT-SOFC Condensed Matter Optical and Electronic Materials Renewable Energy Sources Electrochemistry
Content Type	Text
Resource Type	Article
Subject	Physics and Astronomy Engineering Materials Science Chemical Engineering

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