NDLI: Quantitative analysis of lead in aqueous solutions by ultrasonic nebulizer assisted laser induced breakdown spectroscopy

Content Provider	Springer Nature Link
Author	Zhong, Shi Lei Lu, Yuan Kong, Wei Jin Cheng, Kai Zheng, Ronger
Copyright Year	2016
Abstract	In this study, an ultrasonic nebulizer unit was established to improve the quantitative analysis ability of laser-induced breakdown spectroscopy (LIBS) for liquid samples detection, using solutions of the heavy metal element Pb as an example. An analytical procedure was designed to guarantee the stability and repeatability of the LIBS signal. A series of experiments were carried out strictly according to the procedure. The experimental parameters were optimized based on studies of the pulse energy influence and temporal evolution of the emission features. The plasma temperature and electron density were calculated to confirm the LTE state of the plasma. Normalizing the intensities by background was demonstrated to be an appropriate method in this work. The linear range of this system for Pb analysis was confirmed over a concentration range of 0–4,150ppm by measuring 12 samples with different concentrations. The correlation coefficient of the fitted calibration curve was as high as 99.94% in the linear range, and the LOD of Pb was confirmed as 2.93ppm. Concentration prediction experiments were performed on a further six samples. The excellent quantitative ability of the system was demonstrated by comparison of the real and predicted concentrations of the samples. The lowest relative error was 0.043% and the highest was no more than 7.1%.
Starting Page	1
Ending Page	9
Page Count	9
File Format	PDF
ISSN	20950462
Journal	Frontiers of Physics
Volume Number	11
Issue Number	4
e-ISSN	20950470
Language	English
Publisher	Higher Education Press
Publisher Date	2016-02-02
Publisher Institution	Chinese Universities
Publisher Place	Beijing
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	laser-induced breakdown spectroscopy (LIBS) ultrasonic nebulizer quantitative analysis water solution plasma diagnostics Atomic, Molecular, Optical and Plasma Physics Condensed Matter Physics Particle and Nuclear Physics Astronomy, Astrophysics and Cosmology
Content Type	Text
Resource Type	Article
Subject	Physics and Astronomy

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

The role of microwaves in the enhancement of laser-induced plasma emission

Laser-induced breakdown spectroscopy in Asia

Characterization of laser-induced plasma and application to surface-assisted LIBS for powder and liquid samples

Review of methodological and experimental LIBS techniques for coal analysis and their application in power plants in China

Characterization of the globular oxide inclusion ratings in steel using laser-induced breakdown spectroscopy

Laser-induced breakdown spectroscopy in China

Generation and expansion of laser-induced plasma as a spectroscopic emission source

Quantitative analysis of ITO film by laser-induced breakdown spectroscopy

Research progress in Asia on methods of processing laser-induced breakdown spectroscopy data

Quantitative analysis of lead in aqueous solutions by ultrasonic nebulizer assisted laser induced breakdown spectroscopy

Similar Documents

The role of microwaves in the enhancement of laser-induced plasma emission

Laser-induced breakdown spectroscopy in Asia

Characterization of laser-induced plasma and application to surface-assisted LIBS for powder and liquid samples

Review of methodological and experimental LIBS techniques for coal analysis and their application in power plants in China

Characterization of the globular oxide inclusion ratings in steel using laser-induced breakdown spectroscopy

Laser-induced breakdown spectroscopy in China

Generation and expansion of laser-induced plasma as a spectroscopic emission source

Quantitative analysis of ITO film by laser-induced breakdown spectroscopy

Research progress in Asia on methods of processing laser-induced breakdown spectroscopy data

Quantitative analysis of lead in aqueous solutions by ultrasonic nebulizer assisted laser induced breakdown spectroscopy