NDLI: Calibration of GC-FID and IR Spectrometric Methods for Determination of High Boiling Petroleum Hydrocarbons in Environmental Samples

Content Provider	Springer Nature Link
Author	Krupcík, Ján Oswald, Peter Oktavec, Drahomír Armstrong, Daniel W.
Copyright Year	2004
Abstract	Calibration problems connected with the determination of C$_{20}$-C$_{44}$ petroleum hydrocarbons by gas chromatography – flame ionization detection (GC-FID) and IR spectrometric methods were studied in this paper. It has been found that the mass responses and mass response factors of FID determined by capillary GC-FID as well as by IR spectrometry, at wave number 2959 and 2924 cm$^{-1}$, of high boiling petroleum distillation fractions (in the range C$_{20}$-C$_{46}$) are not constant. Moreover, it was found that mass response factors for differentpetroleum oils that have the same boiling temperature interval might differ up to 1.5 fold both for FID and IRD methods, dependingon their hydrocarbon group composition. However, calibration of the IR spectrometric method using the empirical equations proposed in DIN 38 409, Part 18, norm (for the determination of total petroleumhydrocarbons in waters polluted with high boiled petroleum fractions)gave results which overlapped within ±10% of the expected values.
Starting Page	329
Ending Page	341
Page Count	13
File Format	PDF
ISSN	00496979
Journal	Water, Air, and Soil Pollution
Volume Number	153
Issue Number	1-4
e-ISSN	15732932
Language	English
Publisher	Kluwer Academic Publishers
Publisher Date	2004-01-01
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Hydrogeology Atmospheric Protection/Air Quality Control/Air Pollution
Content Type	Text
Resource Type	Article
Subject	Ecological Modeling Environmental Chemistry Pollution Environmental Engineering Water Science and Technology

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