NDLI: Nanoscale Optimization and Statistical Modeling of Photoelectrochemical Water Splitting Efficiency of N-Doped TiO$

Content Provider	Springer Nature Link
Author	Isimjan, Tayirjan T. Trifkovic, Milana Abdullahi, Inusa Rohani, Sohrab Ray, Ajay K.
Copyright Year	2014
Abstract	Highly ordered nitrogen-doped titanium dioxide (N-doped TiO$_{2}$) nanotube array films with enhanced photo-electrochemical water splitting efficiency (PCE) for hydrogen generation were fabricated by electrochemical anodization, followed by annealing in a nitrogen atmosphere. Morphology, structure and composition of the N-doped TiO$_{2}$ nanotube array films were investigated by FE-SEM, XPS, UV–Vis and XRD. The effect of annealing temperature, heating rate and annealing time on the morphology, structure, and photo-electrochemical property of the N-doped TiO$_{2}$ nanotube array films were investigated. A design of experiments method was applied in order to minimize the number of experiments and obtain a statistical model for this system. From the modelling results, optimum values for the influential factors were obtained in order to achieve the maximum PCE. The optimized experiment resulted in 7.42 % PCE which was within 95 % confidence interval of the predicted value by the model.
Starting Page	114
Ending Page	122
Page Count	9
File Format	PDF
ISSN	10225528
Journal	Topics in Catalysis
Volume Number	58
Issue Number	2-3
e-ISSN	15729028
Language	English
Publisher	Springer US
Publisher Date	2014-12-19
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	TiO$_{2}$ nanotubes Photoelectrochemical water splitting efficiency (PCE) UV irradiation Anodization Design of experiments (DOE) Optimization Catalysis Physical Chemistry Pharmacy Industrial Chemistry/Chemical Engineering Characterization and Evaluation of Materials
Content Type	Text
Resource Type	Article
Subject	Chemistry Catalysis

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