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  1. Russian Journal of General Chemistry
  2. Russian Journal of General Chemistry : Volume 83
  3. Russian Journal of General Chemistry : Volume 83, Issue 10, October 2013
  4. Preparation of 4-nitrostyrene
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Russian Journal of General Chemistry : Volume 87
Russian Journal of General Chemistry : Volume 86
Russian Journal of General Chemistry : Volume 85
Russian Journal of General Chemistry : Volume 84
Russian Journal of General Chemistry : Volume 83
Russian Journal of General Chemistry : Volume 83, Issue 13, December 2013
Russian Journal of General Chemistry : Volume 83, Issue 12, December 2013
Russian Journal of General Chemistry : Volume 83, Issue 11, November 2013
Russian Journal of General Chemistry : Volume 83, Issue 10, October 2013
The solvent influence on some physicochemical properties of Cu(NO$_{3}$)$_{2}$·3H$_{2}$O-(CH$_{3}$)$_{2}$SO solutions
Stability of hydroxyapatite-TiO$_{2}$-Ti structures in physiological solutions of KH$_{2}$PO$_{4}$-Na$_{2}$HPO$_{4}$ at varied pH
Features of the sol-gel process of formation of nanostructured gadolinium oxide
Electron transfer from semiquinone radicals to copper and iron ions
Elementary stages and kinetics of phenoxide radicals reactions with cobalt and iron ions
Study of geometry and electronic structure of molecules, cation-radicals, and anion-radicals of nitromethane, dimethylnitramine, and ethyl nitrate
Quantum-chemical study of thermodynamics of ethylene carbonate reactions with methanol
Bromination of 6-dibromomethyl-6-methylcyclohexyl-2,4-dien-1-one
Reaction of Carbodiimides with trifluoromethanesulfonic acid
Preparation of 4-nitrostyrene
Synthesis, structure and chemical transformations of 4-aminobenzaldehyde
Synthesis and studies of structure and biological properties of D-homoanalogs of steroid estrogens
Catalytic hydrogenation of substituted 15β-Pregn-16-enes
Spatial and electronic structure and $^{35}$Cl NQR parameters of ethyl(trichlorogermyl) propionate according to Ab initio calculations
Acyloxy derivatives of trivalent phosphorus in amidoalkylation of hydrophosphoryl compounds
Radical addition of secondary phosphine chalcogenides to allylamine: Atom-economic synthesis of aminopropylphosphine chalcogenides
Synthesis and properties of triphenylantimony(V) dithiolate derivative
Luminescent and photochemical properties of the lanthanide-containing polymer materials
Synthesis and spectral characteristics of water-soluble pyridine-containing phthalocyanines of cation type
Synthesis of volatile copper(II) β-diketonates, β-ketiminates, and β-diiminates. The problem of synthesis of copper(II) Bis(2,2,6,6-tetramethyl-3-methylaminoheptane-5-onate)
Transition metal complexes with 2,6-Di-tert-butyl-p-quinone 1′-phthalazinylhydrazone
Molecular structure of the macrocyclic copper(II) chelate with 6,7,13,14-tetramethyl-3,10-dithio-1,2,4,5,8,9,11,12-octaazatetradecatetraene-1,5,7,11 according to quantum-chemical DFT calculations
Preparation and spectral properties of Zn(II) complexes with aryl-substituted dipyrrolylmethene and azadipyrrolylmethene
Protolytic dissociation of copper(II) and nickel(II) dipyrrolylmethenates in benzene solutions of acetic acid
Synthesis of 1-(3-Phenoxyphenyl)butane-1,3-dione from ethyl acetoacetate
Synthesis of heterocyclic 1,4-diamino-2,3-dibromo-2-butenes
Reactions of 2-(N,N-dialkyl)amino-2-adamantylcarbonitriles with Grignard reagents
Synthesis and some reactions of 2-[4-(2-chlorobenzyl)-6,6-dimethyltetrahydropyran-4-yl]ethylamine
Reactions of acetyl iodide with triethylsilylalkyl propyl sulfides
Phosphorus-containing azomethines based on salicylaldehyde and thiosemicarbazide
Erratum to: “1-Acyloxygermatranes”
Russian Journal of General Chemistry : Volume 83, Issue 9, September 2013
Russian Journal of General Chemistry : Volume 83, Issue 8, August 2013
Russian Journal of General Chemistry : Volume 83, Issue 7, July 2013
Russian Journal of General Chemistry : Volume 83, Issue 6, June 2013
Russian Journal of General Chemistry : Volume 83, Issue 5, May 2013
Russian Journal of General Chemistry : Volume 83, Issue 4, April 2013
Russian Journal of General Chemistry : Volume 83, Issue 3, March 2013
Russian Journal of General Chemistry : Volume 83, Issue 2, February 2013
Russian Journal of General Chemistry : Volume 83, Issue 1, January 2013
Russian Journal of General Chemistry : Volume 82
Russian Journal of General Chemistry : Volume 81
Russian Journal of General Chemistry : Volume 80
Russian Journal of General Chemistry : Volume 79
Russian Journal of General Chemistry : Volume 78
Russian Journal of General Chemistry : Volume 77
Russian Journal of General Chemistry : Volume 76
Russian Journal of General Chemistry : Volume 75
Russian Journal of General Chemistry : Volume 74
Russian Journal of General Chemistry : Volume 73
Russian Journal of General Chemistry : Volume 72
Russian Journal of General Chemistry : Volume 71

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Preparation of 4-nitrostyrene

Content Provider Springer Nature Link
Author Shultsev, A. L.
Copyright Year 2013
Abstract The interaction of D,L-1-(4-nitrophenyl)ethanol with SOCl$_{2}$ and P$_{4}$O$_{10}$ has been studied. In the reaction of D,L-1-(4-nitrophenyl)ethanol with SOCl$_{2}$ a mixture of 1-(4-nitrophenyl)-1-chloroethane, 1,1′-bis-(4-nitrophenyl)diethyl ether, and 4-nitrostyrene (yield 21%) has been formed. The direction of reaction of D,L-1-(4-nitrophenyl)ethanol with P$_{4}$O$_{10}$ in toluene has been affected significantly by the order of reagents addition and the solution concentration. 4-Nitrostyrene has been obtained in the only case: the addition of P$_{4}$O$_{10}$ to diluted solution of D,L-1-(4-nitrophenyl)ethanol and subsequent refluxing. Also the procedure of 4-nitrostyrene preparation via the cleavage of 2-(4-nitrophenyl)ethyl nitrate with alkoxy anion in the alcoholic solution has been upgraded.
Starting Page 1859
Ending Page 1863
Page Count 5
File Format PDF
ISSN 10703632
Journal Russian Journal of General Chemistry
Volume Number 83
Issue Number 10
e-ISSN 16083350
Language English
Publisher Springer US
Publisher Date 2013-11-14
Publisher Place Boston
Access Restriction One Nation One Subscription (ONOS)
Subject Keyword Chemistry/Food Science
Content Type Text
Resource Type Article
Subject Chemistry
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