NDLI: Anodic fluorination of azobenzene

Content Provider	Springer Nature Link
Author	Kagramav, N. D. Sterlin, S. R. Grinberg, V. A.
Copyright Year	2009
Abstract	Electrolysis of azobenzene (I) in the system of Et$_{4}$NF · 3HF, MeCN results in predominant fluorination of the products of polymerization of I formed in the course of electrolysis. Also, m-fluoroazobenzene (II) and o-fluoroazobenzene (III) (II: III = 4: 1) were obtained with a low yield. Anomalously high content of m-isomer II is probably related to redistribution of localization of electron-deficient centers in cation-radical I as a result of its protonation by acidic electrolyte.
Starting Page	1306
Ending Page	1309
Page Count	4
File Format	PDF
ISSN	10231935
Journal	Russian Journal of Electrochemistry
Volume Number	45
Issue Number	11
e-ISSN	16083342
Language	English
Publisher	SP MAIK Nauka/Interperiodica
Publisher Date	2009-12-06
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	azobenzene tetraethylammoniumfluoride tris-fluorohydrate electrolysis m-fluoroazobenzene o-fluoroazobenzene Physical Chemistry Electrochemistry
Content Type	Text
Resource Type	Article
Subject	Electrochemistry

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Anodic fluorination of azobenzene