NDLI: Synthesis and characterization of MoO$_{3}$ nanostructures by solution combustion method employing morphology and size control

Content Provider	Springer Nature Link
Author	Parviz, D. Kazemeini, M. Rashidi, A. M. Jafari Jozani, Kh.
Copyright Year	2009
Abstract	Molybdenum oxide nanostructures were synthesized utilizing the solution combustion method where the ammonium molybdate powder and an organic additive were used as precursors. Different organic additives including ethylene diamine tetra-acetic acid (EDTA), polyethylene glycol 200 (PEG 200), sorbitol and urea were used as surfactants in order to investigate the effect of additive structure on morphology and particle size of products. Also various reaction parameters such as the additive/Mo molar ratio, concentration of metal ion in solution, pH of the reaction, and temperature of the synthesis media were changed to study effects on product morphology and size. Outcomes were characterized by Scanning Electron Microscopy (SEM), X-ray diffraction, and Transmission Electron Microscopy (TEM) techniques. Results show a variety of MoO$_{3}$ nanoparticles and nanorods produced within the size range of 10–80 nm. Furthermore, microrods and microsheets were also obtained through this method whose length varied in the order of microns.
Starting Page	1509
Ending Page	1521
Page Count	13
File Format	PDF
ISSN	13880764
Journal	Journal of Nanoparticle Research
Volume Number	12
Issue Number	4
e-ISSN	1572896X
Language	English
Publisher	Springer Netherlands
Publisher Date	2009-08-14
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Molybdenum oxide Nanostructures Electron microscopy Optics, Optoelectronics, Plasmonics and Optical Devices Physical Chemistry Inorganic Chemistry Characterization and Evaluation of Materials Nanotechnology
Content Type	Text
Resource Type	Article
Subject	Chemistry Nanoscience and Nanotechnology Atomic and Molecular Physics, and Optics Condensed Matter Physics Bioengineering Modeling and Simulation

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